1,1,1-三溴-2,2,2-三氟乙烷合成路线 （共 16 条）
反应条件
water; hydrogen cation; zinc in N,N-dimethyl-formamide 6 h; irradiated by ultrasound;
参考文献
Journal of Fluorine Chemistry, , vol. 34, p. 241
反应条件
sodium dithionite; hydrazinium monoacetate; sodium hydrogencarbonate 1.) CH3CN, H2O, 0 deg C, 0.5 h, 2.) C2H5OH, reflux, 10 h; Yield given. Multistep reaction;
参考文献
Tang, Xiao-Qing; Hu, Chang-Ming
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 15 p. 2161 - 2164
反应条件
ammonium hydroxide; copper(l) chloride in dimethyl sulfoxide T=20°C; 24 h; Title compound not separated from byproducts;
参考文献
Nenajdenko, Valentine G.; Varseev, Georgy N.; Shastin, Alexey V.; Balenkova, Elisabeth S.
Journal of Fluorine Chemistry, 2005 , vol. 126, # 6 p. 907 - 913
反应条件
ammonium hydroxide; copper(l) chloride in dimethyl sulfoxide
T=20°C; 24 h; Title compound not separated from byproducts;
参考文献
Nenajdenko, Valentine G.; Varseev, Georgy N.; Shastin, Alexey V.; Balenkova, Elisabeth S.
Journal of Fluorine Chemistry, 2005 , vol. 126, # 6 p. 907 - 913
反应条件
ammonium hydroxide; copper(l) chloride in dimethyl sulfoxide
T=20°C; 24 h; Title compound not separated from byproducts;
参考文献
Nenajdenko, Valentine G.; Varseev, Georgy N.; Shastin, Alexey V.; Balenkova, Elisabeth S.
Journal of Fluorine Chemistry, 2005 , vol. 126, # 6 p. 907 - 913
反应条件
ammonium hydroxide; copper(l) chloride in dimethyl sulfoxide
T=20°C; 24 h;
参考文献
Nenajdenko, Valentine G.; Varseev, Georgy N.; Shastin, Alexey V.; Balenkova, Elisabeth S.
Journal of Fluorine Chemistry, 2005 , vol. 126, # 6 p. 907 - 913
