1-氯-1,2-二溴-1,2,2-三氟乙烷合成路线 (共 28 条)
参考文献
Tayouo, Russell; David, Ghislain; Ameduri, Bruno; Boutevin, Bernard
Revue Roumaine de Chimie, 2009 , vol. 54, # 7 p. 545 - 548
反应条件
bromine T=50°C; Product distribution / selectivity;
参考文献
WO2006/26400 A1, ;
Page/Page column 16 ;
反应条件
bromine im UV-Licht;
参考文献
Journal of the Chemical Society, , p. 4423,4429
反应条件
benzophenone; Iodine bromide in dichloromethane T=23°C; 14 h; Irradiation; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 93, # 2 p. 117 - 127
反应条件
bromine; iodine 1.) irradiation, 18-30 deg C, 8 d, 2.) 112 deg C, 112 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 73, # 1 p. 87 - 94
参考文献
Journal of the Chemical Society, , p. 4423,4429
反应条件
sodium hydride; triethylamine in N,N-dimethyl-formamide T=-5°C; 6 h;
参考文献
Tetrahedron Letters, , vol. 28, # 32 p. 3699 - 3702
反应条件
hydrazine hydrate; anhydrous copper acetate in isopropyl alcohol T=30°C; P=22800 Torr; 4 h;
参考文献
Igumnov, Sergei M.; Don, Veronika L.; Vyazkov, Vladimir A.; Narinyan, Karen E.
Mendeleev Communications, 2006 , # 3 p. 189 - 190
反应条件
(NH4)2S2O8; sodium formate in N,N-dimethyl-formamide T=15°C; 20 h;
参考文献
Hu, Chang-Ming; Qing, Feng-Ling; Zhang, Hong-Gen
Journal of Fluorine Chemistry, 1990 , vol. 49, # 2 p. 275 - 280
反应条件
sodium amalgam; sulfuric acid T=60 - 65°C;
参考文献
Farbenfabr.Bayer
Patent: DE952713 , 1956 ;