1,1,1-三氯三氟乙烷合成路线 （共 127 条）
反应条件
ethylenediamine; copper(l) chloride in ethanol T=20°C; 24 h;
参考文献
Nenaidenko; Korotchenko; Shastin; Tyurin; Balenkova
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 12 p. 1750 - 1756
反应条件
Cu2Cl2; ethylenediamine in ethanol T=20°C; Title compound not separated from byproducts;
参考文献
Korotchenko, Vasily N; Shastin, Alexey V; Nenajdenko, Valentine G; Balenkova, Elisabeth S
Tetrahedron, 2001 , vol. 57, # 35 p. 7519 - 7527
反应条件
aluminum oxide; dichloro difluoro methane T=319.85°C; Product distribution; Further Variations:Temperatures;
参考文献
Bozorgzadeh; Kemnitz; Nickkho-Amiry; Skapin; Winfield
Journal of Fluorine Chemistry, 2001 , vol. 107, # 1 p. 45 - 52
反应条件
aluminum oxide; dichloro difluoro methane T=319.85°C; Product distribution; Further Variations:Temperatures;
参考文献
Bozorgzadeh; Kemnitz; Nickkho-Amiry; Skapin; Winfield
Journal of Fluorine Chemistry, 2001 , vol. 107, # 1 p. 45 - 52
反应条件
Cu2Cl2; ethylenediamine in ethanol T=20°C; Title compound not separated from byproducts;
参考文献
Korotchenko, Vasily N; Shastin, Alexey V; Nenajdenko, Valentine G; Balenkova, Elisabeth S
Tetrahedron, 2001 , vol. 57, # 35 p. 7519 - 7527
参考文献
Laurent; Lesniak
Tetrahedron Letters, 1992 , vol. 33, # 52 p. 8091 - 8092
反应条件
aluminium; mercury dichloride in N,N-dimethyl-formamide T=25 - 30°C; 2.5 h;
参考文献
Zeifman, Yu. V.; Postovoi, S. A.; German, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 9.2 p. 1916
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 9 p. 2159 - 2160
反应条件
sodium dithionite; hydrazinium monoacetate; sodium hydrogencarbonate 1.) CH3CN, H2O, 0 deg C, 0.5 h, 2.) C2H5OH, reflux, 10 h; Yield given. Multistep reaction;
参考文献
Tang, Xiao-Qing; Hu, Chang-Ming
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 15 p. 2161 - 2164
参考文献
Kolomeitsev, Alexander; Goerg, Michaela; Dieckbreder, Uwe; Lork, Enno; Roeschenthaler, Gerd-Volker
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 109, # 1-4 p. 597 - 600
参考文献
Kolomeitsev, Alexander; Goerg, Michaela; Dieckbreder, Uwe; Lork, Enno; Roeschenthaler, Gerd-Volker
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 109, # 1-4 p. 597 - 600
