1,1,1-三氯三氟乙烷合成路线 （共 127 条）
反应条件
Cu2Cl2; ethylenediamine in ethanol T=20°C; Title compound not separated from byproducts;
参考文献
Korotchenko, Vasily N; Shastin, Alexey V; Nenajdenko, Valentine G; Balenkova, Elisabeth S
Tetrahedron, 2001 , vol. 57, # 35 p. 7519 - 7527
反应条件
1: 4-chlorobenzaldehyde With hydrazine hydrate in ethanol 2: 1,1,1-trichloro-2,2,2-trifluoro-ethane With ethylenediamine; copper(l) chloride in ethanol T=5 - 20°C; Further stages.;
参考文献
Muzalevskiy; Shastin; Balenkova; Nenajdenko
Russian Chemical Bulletin, 2007 , vol. 56, # 8 p. 1526 - 1533
反应条件
ethylenediamine; copper(l) chloride in ethanol T=20°C; 24 h;
参考文献
Nenaidenko; Korotchenko; Shastin; Tyurin; Balenkova
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 12 p. 1750 - 1756
反应条件
ethylenediamine; copper(l) chloride in ethanol T=20°C; 24 h;
参考文献
Nenaidenko; Korotchenko; Shastin; Tyurin; Balenkova
Russian Chemical Bulletin, 2003 , vol. 52, # 8 p. 1835 - 1840
反应条件
in tetrahydrofuran T=-78 - -50°C;
参考文献
Kolomeitsev, Alexander; Shtarev, Alexander; Chabanenko, Kyrill; Savina, Tatjana; Yagupolskii, Yurii; Goerg, Michaela; Przyborowski, Jan; Lork, Enno; Roeschenthaler, Gerd-Volker
Chemical Communications, 1998 , # 6 p. 705 - 706
反应条件
in tetrahydrofuran Ambient temperatureelectrolyses in undivided cell, Mg anode, stainless steel cathode, NBu4BF4 and NBu4I as supporting electrolyte;
参考文献
Nedelec, J. Y.; Ait-Haddou-Mouloud, H.; Folest, J. C.; Perichon, J.
Tetrahedron Letters, 1988 , vol. 29, # 14 p. 1699 - 1700
参考文献
Kolomeitsev, Alexander; Goerg, Michaela; Dieckbreder, Uwe; Lork, Enno; Roeschenthaler, Gerd-Volker
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 109, # 1-4 p. 597 - 600
反应条件
acetic anhydride; zinc in N,N-dimethyl-formamide T=50°C; 7 h;
参考文献
Li, Chun-Lin; Zhang, Xing-Guo; Tang, Ri-Yuan; Zhong, Ping; Li, Jin-Heng
Journal of Organic Chemistry, 2010 , vol. 75, # 20 p. 7037 - 7040
反应条件
aluminium trifluoride; hydrogen fluoride
T=440°C;
参考文献
Henne; Ruh
Journal of the American Chemical Society, 1948 , vol. 70, p. 1025
反应条件
aluminum oxide; dichloro difluoro methane
T=319.85°C; Product distribution; Further Variations:Temperatures;
参考文献
Bozorgzadeh; Kemnitz; Nickkho-Amiry; Skapin; Winfield
Journal of Fluorine Chemistry, 2001 , vol. 107, # 1 p. 45 - 52
