1,1,1-三氯三氟乙烷合成路线 （共 127 条）
参考文献
Allied Chem. and Dye Corp.
Patent: US2748177 , 1951 ;
反应条件
chloro-trimethyl-silane in N,N-dimethyl-formamide
20 mF, Pt anode; other aldehydes, other halofluoro compounds;
参考文献
Shono; Kise; Oka
Tetrahedron Letters, 1991 , vol. 32, # 45 p. 6567 - 6570
反应条件
in tetrahydrofuran
T=-78 - -50°C;
参考文献
Kolomeitsev, Alexander; Shtarev, Alexander; Chabanenko, Kyrill; Savina, Tatjana; Yagupolskii, Yurii; Goerg, Michaela; Przyborowski, Jan; Lork, Enno; Roeschenthaler, Gerd-Volker
Chemical Communications, 1998 , # 6 p. 705 - 706
参考文献
Kolomeitsev, Alexander; Goerg, Michaela; Dieckbreder, Uwe; Lork, Enno; Roeschenthaler, Gerd-Volker
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 109, # 1-4 p. 597 - 600
反应条件
Cu2Cl2; ethylenediamine in ethanol
T=20°C;
参考文献
Korotchenko, Vasily N; Shastin, Alexey V; Nenajdenko, Valentine G; Balenkova, Elisabeth S
Tetrahedron, 2001 , vol. 57, # 35 p. 7519 - 7527
反应条件
Cu2Cl2; ethylenediamine in ethanol
T=20°C; Title compound not separated from byproducts;
参考文献
Korotchenko, Vasily N; Shastin, Alexey V; Nenajdenko, Valentine G; Balenkova, Elisabeth S
Tetrahedron, 2001 , vol. 57, # 35 p. 7519 - 7527
反应条件
Cu2Cl2; ethylenediamine in ethanol
T=20°C;
参考文献
Korotchenko, Vasily N; Shastin, Alexey V; Nenajdenko, Valentine G; Balenkova, Elisabeth S
Tetrahedron, 2001 , vol. 57, # 35 p. 7519 - 7527
反应条件
Cu-salt in acetonitrile
T=130°C; 14 h;
参考文献
Boutevin, B.; Hervaud, Y.; Pietrasanta, Y.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 20, p. 197 - 206
反应条件
Copper(I)chloride in diethyl ether
参考文献
Montedison S.p.A.
Patent: US4258202 A1, 1981 ;
参考文献
Imperial Chemical Industries Limited
Patent: US4183948 A1, 1980 ;
