1,1,1-三氯三氟乙烷合成路线 （共 127 条）
反应条件
hydrogen T=210°C; 1.5 h; optical yield given as percent de;
参考文献
Stepanov; Delyagina; Cherstkov
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 9 p. 1290 - 1295
反应条件
hydrogen; silica gel; nickel T=449.9°C; P=1 Torr; Product distribution;
参考文献
Chemistry Letters, , # 10 p. 1825 - 1826
反应条件
hydrogenchloride; hydrogen; 5percent Pd/C-H Dehydrochlorination; KineticsActivation energy; Further Variations:Catalysts;
参考文献
Thompson; Rioux; Chen; Ribeiro
Journal of Physical Chemistry B, 2000 , vol. 104, # 14 p. 3067 - 3077
反应条件
hydrogen; Ru/AlF3 T=130 - 150°C; 2 - 24 h;
参考文献
Ausimont S.p.A.
Patent: US6348634 B1, 2002 ;
Location in patent: Page column 4; 5-6 ;
反应条件
UV-Licht.Irradiation;
参考文献
Haszeldine; Nyman
Journal of the Chemical Society, 1959 , p. 387,395
参考文献
Bayer Aktiengesellschaft
Patent: US5536890 A1, 1996 ;
反应条件
hydrogen; silica gel; nickel T=449.9°C; P=1 Torr; Product distribution;
参考文献
Tomioka, Satoshi; Mori, Tohru; Ueda, Wataru; Morikawa, Yutaka; Ikawa, Tsuneo
Chemistry Letters, 1991 , # 10 p. 1825 - 1826
反应条件
1: 1,1,1-trichloro-2,2,2-trifluoro-ethane With zinc in N,N-dimethyl-formamide T=20°C; Metallation; 1 h; 2: carbon dioxide in N,N-dimethyl-formamide Carboxylation; 18 h;
参考文献
Johnson, Theodore R.; Silverman, Richard B.
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 8 p. 1625 - 1636
反应条件
water; hydrogen cation; zinc in N,N-dimethyl-formamide 6 h; irradiated by ultrasound;
参考文献
Hemer,I.; Havlicek,J.
Journal of Fluorine Chemistry, 1986 , vol. 34, p. 241
反应条件
hydrogen; silica gel; nickel T=449.9°C; P=1 Torr; Product distribution;
参考文献
Tomioka, Satoshi; Mori, Tohru; Ueda, Wataru; Morikawa, Yutaka; Ikawa, Tsuneo
Chemistry Letters, 1991 , # 10 p. 1825 - 1826
