1,1,1-三氯三氟乙烷合成路线 (共 127 条)
参考文献
Marangoni, L.; Guglielmo, G.; Conte, L.
Journal of Fluorine Chemistry, 1980 , vol. 16, p. 572
反应条件
UV-Licht.Irradiation;
参考文献
Haszeldine; Nyman
Journal of the Chemical Society, 1959 , p. 387,395
反应条件
hydrogenchloride; hydrogen; 5percent Pd/C-H Dehydrochlorination; KineticsActivation energy; Further Variations:Catalysts;
参考文献
Thompson; Rioux; Chen; Ribeiro
Journal of Physical Chemistry B, 2000 , vol. 104, # 14 p. 3067 - 3077
反应条件
aluminium trichloride; phosphorus trichoride
参考文献
Boutevin, B.; Hervaud, Y.; Pietrasanta, Y.
Phosphorus and Sulfur and the Related Elements, 1981 , vol. 11, p. 373 - 382
反应条件
carbon monoxide in tetrahydrofuran a suspn. of Rh dimer in THF and CF3CCl3 were stirred at room temp. for 16 h under CO atmosphere; chlomy. over Florisil, eluent CHCl3;
参考文献
Booth, Brian L.; Casey, Geoffrey C.; Haszeldine, Robert N.
Journal of Organometallic Chemistry, 1982 , vol. 224, # 2 p. 197 - 205
反应条件
in tetrahydrofuran byproducts: carbon monoxide; mixture was stirred at room temp. for 15 h under CO; chromd. (alumina), recrystd. from CHCl3/EtOH;
参考文献
Booth, Brian L.; Casey, Geoffrey C.; Haszeldine, Robert N.
Journal of Organometallic Chemistry, 1981 , vol. 219, # 3 p. 401 - 408
反应条件
(NH4)2S2O8; sodium formate in N,N-dimethyl-formamide T=25°C; 10 h; different redox systems and solvents; Product distribution;
参考文献
Journal of Fluorine Chemistry, , vol. 49, # 2 p. 275 - 280
反应条件
(NH4)2S2O8 in N,N-dimethyl-formamide T=40°C; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 56, # 8 p. 2801 - 2804
反应条件
acetic anhydride; zinc in N,N-dimethyl-formamide T=50°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Fujita; Kondo; Hiyama
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 12 p. 4385 - 4394
反应条件
hydrogen T=180 - 220°C; optical yield given as percent de;
参考文献
Stepanov; Delyagina; Cherstkov
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 9 p. 1290 - 1295