1,1,1-三氯三氟乙烷合成路线 (共 127 条)
反应条件
hydrogen T=210°C; 1.5 h; optical yield given as percent de;
参考文献
Stepanov; Delyagina; Cherstkov
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 9 p. 1290 - 1295
反应条件
hydrogen T=180°C; 2 h; optical yield given as percent de;
参考文献
Stepanov; Delyagina; Cherstkov
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 9 p. 1290 - 1295
反应条件
hydrogen; Ru/AlF3 T=130 - 150°C; 2 - 24 h;
参考文献
Ausimont S.p.A.
Patent: US6348634 B1, 2002 ;
Location in patent: Page column 4; 5-6 ;
反应条件
hydrogen; 5 wt Ru/carbon T=100 - 130°C; 20 h;
参考文献
Ausimont S.p.A.
Patent: US6348634 B1, 2002 ;
Location in patent: Page column 4-5 ;
反应条件
hydrogen; silica gel; nickel T=449.9°C; P=1 Torr; Product distribution;
参考文献
Chemistry Letters, , # 10 p. 1825 - 1826
反应条件
acetic anhydride; zinc in N,N-dimethyl-formamide T=50°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Fujita; Kondo; Hiyama
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 12 p. 4385 - 4394
参考文献
PCUK Products Chimiques Ugine Kuhlmann
Patent: US4605798 A1, 1986 ;
参考文献
PCUK Products Chimiques Ugine Kuhlmann
Patent: US4605798 A1, 1986 ;
反应条件
aluminium trifluoride; hydrogen fluoride T=445°C;
参考文献
Allied Chem.and Dye Corp.
Patent: US2748177 , 1951 ;
参考文献
Allied Chem. and Dye Corp.
Patent: US2748177 , 1951 ;