1,1,1-三氯三氟乙烷合成路线 （共 127 条）
反应条件
hydrogen; silica gel; nickel T=449.9°C; P=1 Torr; Product distribution;
参考文献
Chemistry Letters, , # 10 p. 1825 - 1826
反应条件
Cu2Cl2; ethylenediamine in ethanol T=20°C; Title compound not separated from byproducts;
参考文献
Korotchenko, Vasily N; Shastin, Alexey V; Nenajdenko, Valentine G; Balenkova, Elisabeth S
Tetrahedron, 2001 , vol. 57, # 35 p. 7519 - 7527
反应条件
(NH4)2S2O8; ammonium formate in N,N-dimethyl-formamide T=30 - 40°C;
参考文献
Hu, Chang-Ming; Tu, Ming-Hu
Journal of Fluorine Chemistry, 1991 , vol. 55, # 1 p. 105 - 108
反应条件
hydrogen; RhCl(PPh3)3 in tetrahydrofuran T=100°C; P=6080 Torr; 5 h; further catalysts and times; effect of bases; Product distribution;
参考文献
Journal of Fluorine Chemistry, , vol. 71, # 1 p. 107 - 110
反应条件
hydrogenchloride; hydrogen; 5percent Pd/C-H Dehydrochlorination; KineticsActivation energy; Further Variations:Catalysts;
参考文献
Thompson; Rioux; Chen; Ribeiro
Journal of Physical Chemistry B, 2000 , vol. 104, # 14 p. 3067 - 3077
反应条件
hydrogen; Pd-Cu [1/1] bimetallic particles T=350°C;
参考文献
US2004/127757 A1, ;
Page 6 ;
反应条件
Cu2Cl2; ethylenediamine in ethanol T=20°C; Title compound not separated from byproducts;
参考文献
Korotchenko, Vasily N; Shastin, Alexey V; Nenajdenko, Valentine G; Balenkova, Elisabeth S
Tetrahedron, 2001 , vol. 57, # 35 p. 7519 - 7527
反应条件
aluminum oxide; dichloro difluoro methane T=319.85°C; Product distribution; Further Variations:Temperatures;
参考文献
Bozorgzadeh; Kemnitz; Nickkho-Amiry; Skapin; Winfield
Journal of Fluorine Chemistry, 2001 , vol. 107, # 1 p. 45 - 52
反应条件
perchloric acid in water Ambient temperature; Rate constant;
参考文献
Schoeneich, Christian; Asmus, Klaus-Dieter; Bonifacic, Marija
Journal of the Chemical Society, Faraday Transactions, 1995 , vol. 91, # 13 p. 1923 - 1930
反应条件
iso-propylmagnesium bromide in diethyl ether 1.) -70 deg C, 30 min; 2.) -70 deg C, 2 h then up to RT, 2 h;
参考文献
Hemer,I.; Posta,A.
Journal of Fluorine Chemistry, 1984 , vol. 26, p. 467
