1,2-二氯-2-碘-1,1,2-三氟乙烷合成路线 (共 50 条)
反应条件
acetic anhydride; zinc in dichloromethane T=40°C;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 73, # 12 p. 1719 - 1728
反应条件
cadmium in acetonitrile 1 h; Ambient temperature;
参考文献
Journal of Fluorine Chemistry, , vol. 36, p. 123 - 140
参考文献
Miller et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 4159,4163
Full Text Show Details
Haszeldine
Journal of the Chemical Society, 1952 , p. 4423,4429
参考文献
Haszeldine
Journal of the Chemical Society, 1952 , p. 4423,4429
参考文献
Haszeldine
Journal of the Chemical Society, 1952 , p. 4423,4429
参考文献
Haszeldine
Journal of the Chemical Society, 1952 , p. 4423,4429
反应条件
1: With zinc in ethyl acetate T=20°C; 41 h; 2: With zinc in isopropyl alcohol T=80°C; 2 h;
参考文献
Karimova; Glazkov; Ignatenko; Mysova
Russian Chemical Bulletin, 2004 , vol. 53, # 10 p. 2336 - 2337
反应条件
acetic anhydride; zinc 1.) ethylene chloride, 16 deg C, 5 h, 2.) ethanol, reflux; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 25, # 12.2 p. 2316 - 2320
Zhurnal Organicheskoi Khimii, , vol. 25, # 12 p. 2582 - 2588
反应条件
sodium dithionite; sodium hydrogencarbonate in water; acetonitrile T=40°C; 4 h;
参考文献
Gorbunova, T. I.; Kodess, M. I.; Podol'skii, A. V.; Saloumin, V. I.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 10 p. 2364 - 2365,2194 - 2195
反应条件
Irradiation.bei der Bestrahlung mit UV-Licht und Behandlung des Reaktionsprodukts mit Chlor in 1,1,2-Trichlor-1,2,2-trifluor-aethan im UV-Licht;
参考文献
Haszeldine
Journal of the Chemical Society, 1955 , p. 4291,4300
Full Text Show Details
Kellog Co.
Patent: US2742510 , 1955 ;