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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
五氟碘乙烷
合成路线
（共 188 条）
354-64-3
五氟碘乙烷
+
80937-33-3
→
反应条件
353-50-4
氟光气
+
354-34-7
三氟乙酰氟
+
7553-56-2
碘
+
7783-61-1
四氟化硅
+
7782-41-4
氟
反应条件
Kinetics; Irradiation (UV/VIS); photochemical oxidn., ambient temp.;
参考文献
Marsh; Heicklen
Journal of Physical Chemistry, 1966 , vol. 70, p. 3008
Full Text View citing articles Show Details
Gmelin Handbook: C: MVol.D3, 2.1.1.10, page 19 - 20
354-64-3
五氟碘乙烷
+
661-69-8
六甲基二锡
→
反应条件
594-27-4
四甲基锡
+
811-73-4
三甲基碘锡烷
+
812-35-1
反应条件
in neat (no solvent) Irradiation (UV/VIS); UV-irradiation of a mixt. of ((CH3)3Sn)2 and C2F5I for 24 h;;
参考文献
Cullen et al.
Inorganic Chemistry, 1970 , vol. 9, p. 1682,1683, 1684
Full Text View citing articles Show Details
Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.1.3, page 31 - 41
354-64-3
五氟碘乙烷
+
661-69-8
六甲基二锡
→
反应条件
594-27-4
四甲基锡
反应条件
Irradiation (UV/VIS);
参考文献
Cullen et al.
Inorganic Chemistry, 1970 , vol. 9, p. 1682,1683, 1684
116-14-3
四氟乙烯
+
54509-73-8
+
354-64-3
五氟碘乙烷
+
10192-85-5
丙烯酸钾
→
反应条件
34395-24-9
2-(全氟十二烷基)乙基丙烯酸酯
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 8-9 ;
354-64-3
五氟碘乙烷
→
反应条件
116-14-3
四氟乙烯
+
76-19-7
八氟丙烷
+
2314-97-8
+
76-16-4
+
355-25-9
反应条件
T=22°C; P=0.5 Torr; infrared multiphoton dissociation; variation of frequency and fluence; Product distribution;
参考文献
Weinberg, E.; Gauthier, M.; Hackett, P. A.; Willis, C.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 1307 - 1310
116-14-3
四氟乙烯
+
54509-73-8
+
354-64-3
五氟碘乙烷
+
10192-85-5
丙烯酸钾
→
反应条件
865-86-1
+
21652-58-4
+
678-39-7
+
30389-25-4
+
27905-45-9
+
17741-60-5
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 9 ;
116-14-3
四氟乙烯
+
54509-73-8
+
354-64-3
五氟碘乙烷
+
10192-85-5
丙烯酸钾
→
反应条件
34395-24-9
2-(全氟十二烷基)乙基丙烯酸酯
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 8-9 ;
116-14-3
四氟乙烯
+
54509-73-8
+
354-64-3
五氟碘乙烷
+
10192-85-5
丙烯酸钾
→
反应条件
34395-24-9
2-(全氟十二烷基)乙基丙烯酸酯
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 9-10 ;
116-14-3
四氟乙烯
+
54509-73-8
+
354-64-3
五氟碘乙烷
+
10192-85-5
丙烯酸钾
→
反应条件
865-86-1
+
21652-58-4
+
678-39-7
+
30389-25-4
+
27905-45-9
+
17741-60-5
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 9 ;
116-14-3
四氟乙烯
+
54509-73-8
+
354-64-3
五氟碘乙烷
+
10192-85-5
丙烯酸钾
→
反应条件
34395-24-9
2-(全氟十二烷基)乙基丙烯酸酯
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 8-9 ;
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