反应条件
CH3Li in diethyl ether mixing ethereal soln. of perfluoroethyl iodide and ethereal soln. of methyllithium, addn. to ethreal soln. of tin compd.; reaction were conducted at -68°C in system of micromixers, microreactors and tube precooling units; quenching with methanol, treatment with aq. NaHCO3, GC;
参考文献
Nagaki, Aiichiro; Tokuoka, Shinya; Yamada, Shigeyuki; Tomida, Yutaka; Oshiro, Kojun; Amii, Hideki; Yoshida, Jun-Ichi
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 21 p. 7559 - 7563
