1,1,1,2,3,4,4,4-八氟-2,3-二(三氟甲基)丁烷合成路线 （共 22 条）
反应条件
lithium in diethylene glycol -45°C for 4 h, then keeping at room temp. overnight;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.2.7.1, page 104 - 132
反应条件
cesium fluoride T=215°C; P=10640 Torr; 87 h; Further byproducts given;
参考文献
Dresdner,R.D. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 3524 - 3527
反应条件
PSHF in acetonitrile
参考文献
Chambers, Richard D.; Holmes, Thomas F.; Korn, Stewart R.; Standford, Graham
Journal of the Chemical Society, Chemical Communications, 1993 , # 10 p. 855 - 856
反应条件
acetic anhydride; zinc in dichloromethane T=40°C;
参考文献
Wlassics, Ivan; Tortelli, Vito
Collection of Czechoslovak Chemical Communications, 2008 , vol. 73, # 12 p. 1719 - 1728
反应条件
acetic anhydride; zinc in dichloromethane T=40°C;
参考文献
Wlassics, Ivan; Tortelli, Vito
Collection of Czechoslovak Chemical Communications, 2008 , vol. 73, # 12 p. 1719 - 1728
反应条件
fluorine in various solvent(s) T=5°C; 7 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Tonelli, Claudio; Tortelli, Vito
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 23 - 26
反应条件
cobalt(III) fluoride T=360°C; 3 h; Further byproducts given;
参考文献
Burdon, James; Creasey, Jeremy C.; Proctor, Lee D.; Plevey, Raymond G.; Yeoman, J.R. Neil
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 4 p. 445 - 447
反应条件
cesium fluoride T=350°C; 0.0333333 h;
参考文献
Dresdner,R.D. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 3524 - 3527
反应条件
T=250°C; P=7500.6 Torr; Pyrex tube;
参考文献
Probst, Anton; Werner, Konrad von
Journal of Fluorine Chemistry, 1990 , vol. 47, p. 163 - 173
参考文献
Probst, Anton; Werner, Konrad von
Journal of Fluorine Chemistry, 1990 , vol. 47, p. 163 - 173
