反应条件
ethanol in ethylene glycol dimethyl ether; ethanol to educts added DME-EtOH mixt., kept for 5 min at 20°C; ppt. isolated, soln. evapd., washed with hexane at 0°C, recrystd. from toluene, mother liquor cooled at -78°C for 24 h, ppt. isolated, evapd.;
参考文献
Razuvaev, G. A.; Bochkarev, M. N.; Pankratov, L. V.
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 135 - 144
