反应条件
in tetrahydrofuran byproducts: TlBr; sealed vessel, vac.; addn. of equimolar amt. of germane to Hg-compd. (room temp.); decantation from TlCl, standing overnight at 20°C (pptn.), decantation, washing of digermane (hexane), sublimation (vac.); evapn. of decanted soln., washing of Hg-compd. (hexane), drying (vac.); gas chromy. of (C6F5)3GeH in washings;
参考文献
Bochkarev, M. N.; Gur'ev, N. I.; Pankratov, L. V.; Razuvaev, G. A.
Inorganica Chimica Acta, 1980 , vol. 44, p. L59 - L60
