2,3-二棕榈酰-Sn-甘油-1-磷酰胆碱合成路线 (共 14 条)
反应条件
1: 1.) Et3N, 2.) H2O / 1.) CH2Cl2, 0-5 deg C, 2.) 30 min 2: ethanol; CHCl3 / 70 - 80 °C View Scheme
参考文献
Ishihara, Masami; Sano, Atsunori
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 5 p. 1096 - 1098
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in chloroform; dimethyl sulfoxide T=40°C; 48 h;
参考文献
Tomoi, Masao; Inomata, Kiyoshi; Kakiuchi, Hiroshi; Tokuyama, Satoru
Synthetic Communications, 1989 , vol. 19, # 5and6 p. 907 - 916
反应条件
HEPES buffer in chloroform T=37°C; Bovine Albuminum fraction;
参考文献
Lin; Liu; Wu; Jen
Synthetic Communications, 1993 , vol. 23, # 15 p. 2135 - 2138
反应条件
HEPES buffer in chloroform T=37°C; Bovine Albumin fraction (BSA);
参考文献
Lin; Liu; Wu; Jen
Synthetic Communications, 1993 , vol. 23, # 15 p. 2135 - 2138
反应条件
1: pyridine / CHCl3 / Ambient temperature 2: 10percent aq. NaHCO3 / CHCl3 / Ambient temperature View Scheme
参考文献
Ishihara, Masami; Sano, Atsunori
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 5 p. 1096 - 1098
反应条件
1: 88 percent / BCl3 / CH2Cl2 / 0.5 h / -78 - -40 °C 2: 1.) Et3N, 2.) H2O / 1.) CH2Cl2, 0-5 deg C, 2.) 30 min 3: ethanol; CHCl3 / 70 - 80 °C View Scheme
参考文献
Xia, Jie; Hui, Yong-Zheng
Tetrahedron Asymmetry, 1997 , vol. 8, # 18 p. 3019 - 3021
反应条件
1: dicyclohexylcarbodiimide, DMAP / CH2Cl2 / 12 h / Ambient temperature 2: 88 percent / BCl3 / CH2Cl2 / 0.5 h / -78 - -40 °C 3: 1.) Et3N, 2.) H2O / 1.) CH2Cl2, 0-5 deg C, 2.) 30 min 4: ethanol; CHCl3 / 70 - 80 °C View Scheme
参考文献
Xia, Jie; Hui, Yong-Zheng
Tetrahedron Asymmetry, 1997 , vol. 8, # 18 p. 3019 - 3021
反应条件
in ethanol; chloroform T=70 - 80°C; Yield given;
参考文献
Xia, Jie; Hui, Yong-Zheng
Tetrahedron Asymmetry, 1997 , vol. 8, # 18 p. 3019 - 3021
反应条件
phospholipase A2; HEPES-buffer pH 7.2 in chloroform T=37°C; reaction rate; other acyl donors;
参考文献
Lin, Gialih; Wu, Fang-Chen; Liu, Shih-Huang
Tetrahedron Letters, 1993 , vol. 34, # 12 p. 1959 - 1962
反应条件
phospholipase D-P in chloroform T=45°C; 6 h; 100 mM acetate buffer (pH 4.0);
参考文献
Shuto, Satoshi; Ueda, Shigeru; Imamura, Shigeyuki; Fukukawa, Kiyofumi; Matsuda, Akira; Ueda, Tohru
Tetrahedron Letters, 1987 , vol. 28, # 2 p. 199 - 202