sulfuric acid; hydrogen bromide; sodium nitrite in water T=0 - 5°C; 1 h;
参考文献
Gashev, S. B.; Sedova, V. F.; Smirnov, L. D.; Mamaev, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 1008 - 1012
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1257 - 1261
sodium methylate in methanol T=180°C; 8 h; autoclave;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 19, # 9 p. 1008 - 1012
Khimiya Geterotsiklicheskikh Soedinenii, , # 9 p. 1257 - 1261
sodium methylate in methanol
T=180°C; 8 h; autoclave;
参考文献
Gashev, S. B.; Sedova, V. F.; Smirnov, L. D.; Mamaev, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 1008 - 1012
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1257 - 1261
1: 72 percent / sodium methoxide / methanol / 8 h / 180 °C / autoclave
2: 37 percent / m-chloroperbenzoic acid / acetone / 72 h / 20 °C
View Scheme
参考文献
Gashev, S. B.; Sedova, V. F.; Smirnov, L. D.; Mamaev, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 1008 - 1012
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1257 - 1261
1: 72 percent / sodium methoxide / methanol / 8 h / 180 °C / autoclave
2: 66 percent / chlorobenzene / 0.17 h / Heating
View Scheme
参考文献
Gashev, S. B.; Sedova, V. F.; Smirnov, L. D.; Mamaev, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 1008 - 1012
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1257 - 1261
1: 72 percent / sodium methoxide / methanol / 8 h / 180 °C / autoclave
2: 68 percent / triethylamine / chlorobenzene / 0.17 h / Heating
View Scheme
参考文献
Gashev, S. B.; Sedova, V. F.; Smirnov, L. D.; Mamaev, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 1008 - 1012
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1257 - 1261
1: 72 percent / sodium methoxide / methanol / 8 h / 180 °C / autoclave
2: 72 percent / 10percent ammonium hydroxide, iodine, KI / H2O / 4 h / 45 °C
View Scheme
参考文献
Gashev, S. B.; Sedova, V. F.; Smirnov, L. D.; Mamaev, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 1008 - 1012
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1257 - 1261
1: 72 percent / sodium methoxide / methanol / 8 h / 180 °C / autoclave
2: 37 percent / m-chloroperbenzoic acid / acetone / 72 h / 20 °C
3: 61 percent / triethylamine / benzene / 0.25 h / Heating
View Scheme
参考文献
Gashev, S. B.; Sedova, V. F.; Smirnov, L. D.; Mamaev, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 9 p. 1008 - 1012
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 9 p. 1257 - 1261