4-(2-乙酰氨基基乙基)苯磺酰氯合成路线 (共 3 条)
反应条件
chlorosulfonic acid T=50 - 70°C; 3 h;
参考文献
Ha-Duong; Dijols; Marques-Soares; Minoletti; Dansette; Mansuy
Journal of Medicinal Chemistry, 2001 , vol. 44, # 22 p. 3622 - 3631
反应条件
ammonium hydroxide in water T=20°C; 12 h;
参考文献
Zhang, Hui-bin; Zhang, Ya-an; Wu, Guan-zhong; Zhou, Jin-pei; Huang, Wen-long; Hu, Xiao-wen
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 6 p. 1740 - 1744
反应条件
1: aqueous ammonia 2: aqueous hydrochloric acid View Scheme
参考文献
Miller et al.
Journal of the American Chemical Society, 1940 , vol. 62, p. 2099,2101