2,2,3,3,4,4,5,5-八氟-1-戊醇合成路线 (共 86 条)
反应条件
1: With polyethylsiloxane; LiTi(OPr-i)4 T=100°C; 24 h; 2: With sodium hydroxide in tetrahydrofuran 3 h; Heating;
参考文献
Kozhukhova; Yatluk; Suvorov; Koryakova
Russian Journal of Organic Chemistry, 2004 , vol. 40, # 6 p. 759 - 762
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C;
参考文献
Journal of Medicinal Chemistry, , vol. 56, # 1 p. 73 - 83
反应条件
1,1'-azobis (cyclohexanecarbonitrile) T=125°C;
反应条件
dibenzoyl peroxide T=-30°C; 6 h; Yields of byproduct given;
参考文献
Paleta, O.; Dedek, V.; Reutschek, H.; Timpe, H.-J.
Journal of Fluorine Chemistry, 1989 , vol. 42, p. 345 - 354
反应条件
2,2,2-trichloro-1,1-ethanediol in benzene 10 h; Heating; Yields of byproduct given;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 56, # 12 p. 2696 - 2700,2385 - 2388
反应条件
2,2,2-trichloro-1,1-ethanediol in benzene 12 h; Heating;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 56, # 12 p. 2696 - 2700,2385 - 2388
反应条件
in benzene T=40°C; 8 h;
参考文献
Krutikova; Krutikov; Erkin
Russian Journal of General Chemistry, 2010 , vol. 80, # 3 p. 428 - 433
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 51, # 3 p. 542 - 547,423 - 428
反应条件
1: 81.5 percent / CF3COOH / 5 h / 140 °C 2: 77.8 percent / N2O4 / 10 h / 20 °C 3: 1.4 g / Heating View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 7 p. 1332 - 1334
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1641 - 1643
反应条件
in benzene 10 h; Heating; Yields of byproduct given;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 56, # 12 p. 2696 - 2700,2385 - 2388