2,2,3,3,4,4,5,5-八氟-1-戊醇合成路线 (共 86 条)
反应条件
thionyl chloride T=25°C; 2 h;
参考文献
Rakhimov
Russian Journal of General Chemistry, 2010 , vol. 80, # 8 p. 1626 - 1645
反应条件
thionyl chloride; N,N-dimethyl-formamide
参考文献
Rakhimov
Russian Journal of General Chemistry, 2010 , vol. 80, # 8 p. 1626 - 1645
反应条件
oxygen; vanadium pentoxide; silica gel T=350°C;
参考文献
Kharchuk; Shishmakov; Volkov; Petrov
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 2 p. 284 - 285
反应条件
triethylamine T=5 - 20°C;
参考文献
Studnev, Yu. N.; Kinosh, O. F.; Zabornya, V. V.; Frolovskii, V. A.; Stolyarov, V. P.; Rozantsev, G. G.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.1 p. 1162 - 1163
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1292 - 1293
反应条件
1: 85 percent / aq. KOH / benzene / 1 h / 80 °C 2: 76 percent / KI / bis-(2-hydroxy-ethyl) ether / Heating View Scheme
参考文献
Konno, Tsutomu; Kishi, Misato; Ishihara, Takashi; Yamada, Shigeyuki
Journal of Fluorine Chemistry, 2013 , vol. 156, p. 144 - 151
反应条件
phosphonitrilic chloride trimer; sodium in tetrahydrofuran
参考文献
Gol'din,G.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1976 , vol. 46, p. 688 - 691,685 - 688
反应条件
1: With titanium tetrachloride Inert atmosphere; 2: With zinc in diethylene glycol dimethyl ether T=90°C; 9 h; Cooling with ice;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY; STEPANOV, Andrei, Aleksandrovich; CHERSTKOV, Victor, Filippovich; NAPPA, Mario, Joseph
Patent: WO2011/90734 A1, 2011 ;
Location in patent: Page/Page column 6-7 ;
反应条件
1: 75 percent / triphenylphosphine, bromine / CCl4 / Heating 2: 75 percent / zinc powder / acetic acid / Heating View Scheme
参考文献
DAIKIN INDUSTRIES, LTD.; KOMATSU, Yuzo; SUGIYAMA, Akinari; SHIBANUMA, Takashi
Patent: WO2010/87465 A1, 2010 ;
Location in patent: Page/Page column 13-14 ;
反应条件
in 1,2-dichloro-ethane T=35 - 37°C;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 51, # 12 p. 2711 - 2715,2339 - 2343
反应条件
sodium hydroxide; tetrabutyl-ammonium chloride T=40°C; 8.5 h;
参考文献
Journal of Organometallic Chemistry, , vol. 405, # 2 p. 179 - 182