2,2,3,3,4,4,5,5-八氟-1-戊醇合成路线 （共 86 条）
反应条件
bromine; triphenylphosphine in tetrachloromethane
Heating;
参考文献
Zapevalov, A. Yu.; Saloutina, L. V.; Kodess, M. I.; Kolenko, I. P.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 8 p. 1466 - 1472
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1626 - 1633
反应条件
phosphorus trichloride dibromide in tetrachloromethane
1) -40 deg C, 2 h; 2) 20 deg C, 3 h.;
参考文献
Krolevets, A. A.; Ragulin, L. I.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 4 p. 929 - 930,818
反应条件
chlorine fluorosulfate in 1,2,2-trifluoro-trichloroethane
参考文献
Fokin, A. V; Studnev, Yu. N.; Rapkin, A. I.; Pasevina, K. I.; Potarina, T. M.; Verenikin, O. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, p. 1684 - 1688
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 10 p. 2369 - 2374
反应条件
Cadmium acetate
P=9120 Torr;
参考文献
Trofimov, B. A.; Khil'ko, M. Ya.; Nedolya, N. A.; Demanov, Yu. K.; Vyalykh, E. P.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 647 - 651
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 4 p. 744 - 749
反应条件
1: Et3N / CH2Cl2
View Scheme
参考文献
Gandel'sman,L.Z. et al.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 808 - 809
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, p. 872
反应条件
1: 66 percent / NaOH / H2O / 50 - 65 °C
2: KF, NMP / 6 h / 195 °C
View Scheme
参考文献
Puy, Michael Van Der; Poss, Andrew J.; Persichini, Phillip J.; Ellis, Lois A. S.
Journal of Fluorine Chemistry, 1994 , vol. 67, # 3 p. 215 - 224
反应条件
1: H2SO4 / 110 - 120 °C
2: aq. NaHSO3
View Scheme
参考文献
Gol'din,G.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1977 , vol. 47, # 5 p. 1086 - 1088,995 - 997
参考文献
Brace,N.O.; McCormack,W.B.
Journal of Organic Chemistry, 1961 , vol. 26, p. 5091 - 5099
反应条件
phosphorus tribromide in neat (no solvent)
20 deg C, 1 h, 50-60 deg C, 45 h;
参考文献
Krolevets, A. A.; Ragulin, L. I.; Shevchenko, V. I.; Lyubimova, E. I.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 3 p. 584 - 588,516 - 520
反应条件
1: 85 percent / PCl3, H2O / H2O / 1.5 h / 0 - 10 °C
2: Et3N / 0.67 h / 70 °C
View Scheme
参考文献
Mironov, V. F.; Konovalova, I. V.
Russian Journal of General Chemistry, 1993 , vol. 63, # 10.1 p. 1548 - 1550
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 10 p. 2228 - 2232
