2,2,3,3,4,4,5,5-八氟-1-戊醇合成路线 （共 86 条）
反应条件
phosphorus tribromide
1 h, 20 deg C, then about 45 h, 50-60 deg C; Product distribution;
参考文献
Krolevets, A. A.; Ragulin, L. I.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 2 p. 461 - 462,408 - 409
反应条件
water; phosphorus trichoride in water
T=0 - 10°C; 1.5 h;
参考文献
Mironov, V. F.; Konovalova, I. V.
Russian Journal of General Chemistry, 1993 , vol. 63, # 10.1 p. 1548 - 1550
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 10 p. 2228 - 2232
反应条件
1: bis(trichloromethyl) carbonate With pyridine in pentane
T=-15°C; 1 h;
2: 2,2,3,3,4,4,5,5-octafluoro-1-pentanol in pentane
T=-15°C; 6 h;
参考文献
Vincenti, Marco; Ghiglione, Nicoletta; Valsania, Maria Carmen; Davit, Patrizia; Richardson, Susan D.
Helvetica Chimica Acta, 2004 , vol. 87, # 2 p. 370 - 375
反应条件
aluminium trichloride in tetrachloromethane
T=60 - 70°C; 4 h; Yields of byproduct given;
参考文献
Petrova, T. D.; Ryabichev, A. G.; Savchenko, T. I.; Kolesnikova I. V.; Platonov, V. E.
Journal of Organic Chemistry USSR (English Translation), 1988 , p. 1362 - 1366
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 7 p. 1513 - 1517
反应条件
water; iron(III) chloride
参考文献
Hill,M.E. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 411 - 415
反应条件
tetrachloromethane; iron(III) chloride
参考文献
Hill,M.E. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 411 - 415
反应条件
2: <(CH3)3CO>2 / benzene / 1 h / 130 °C
View Scheme
参考文献
Gizatullina, S. P.; Sokolovskii, A. V.; Germash, A. V.; Zlot-skii, S. S.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. <2> 60, # 11 p. 2565 - 2568,2297 - 2299
参考文献
Brace,N.O.; McCormack,W.B.
Journal of Organic Chemistry, 1961 , vol. 26, p. 5091 - 5099
参考文献
Hill,M.E. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 411 - 415
反应条件
in cyclohexanone
T=70 - 130°C; 4 h; Sonication;
参考文献
Rakhimova; Kudashev
Russian Journal of General Chemistry, 2011 , vol. 81, # 7 p. 1529 - 1534
