2,2'-[硫代羰酰双(硫)]双[2-甲基丙酸]合成路线 (共 2 条)
反应条件
1: carbon disulfide With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in water; toluene T=20°C; 2: chloroform; acetone in water; toluene T=20 - 30°C; 0.5 h; 3: With hydrogenchloride in water
参考文献
NOVEON IP HOLDINGS CORP.
Patent: WO2005/80326 A1, 2005 ;
Location in patent: Page/Page column 33-34 ;
反应条件
1: With Trimethyldecylammonium bromide in hexane; chloroform T=10°C; Inert atmosphere; 2: With sodium hydroxide in hexane; chloroform T=25°C; Inert atmosphere; 3: With hydrogenchloride; water in hexane; chloroform 0.5 h; Inert atmosphere;
参考文献
Tominey, Alan F.; Liese, Julia; Kraft, Arno; Wei, Sun; Kowski, Klaus; Schrader, Thomas
Beilstein Journal of Organic Chemistry, 2010 , vol. 6, art. no. 66