3,5-二-(烯丙氧基)-4-溴苯甲醛合成路线 （共 3 条）
反应条件
Celite; sodium acetate; pyridinium chlorochromate in dichloromethane T=0°C; 4.5 h;
参考文献
President and Fellows of Harvard College; CBR Institute for Biomedical Research, Inc.
Patent: US6797819 B1, 2004 ;
反应条件
1: 47 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / 0 °C 2: 94 percent / pyridinium chlorochromate; celite; sodium acetate / CH2Cl2 / 4.5 h / 0 °C View Scheme
参考文献
Pelish; Westwood; Feng; Kirchhausen; Shair
Journal of the American Chemical Society, 2001 , vol. 123, # 27 p. 6740 - 6741
反应条件
1: 97 percent / K2CO3 / dimethylformamide / 15 h / 20 °C 2: 47 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / 0 °C 3: 94 percent / pyridinium chlorochromate; celite; sodium acetate / CH2Cl2 / 4.5 h / 0 °C View Scheme
参考文献
Pelish; Westwood; Feng; Kirchhausen; Shair
Journal of the American Chemical Society, 2001 , vol. 123, # 27 p. 6740 - 6741
