2,2'-环二氧-2,2'-联金刚烷合成路线 (共 14 条)
反应条件
oxygen; methylene blue T=50°C; 40 h; IrradiationFlorisil support;
参考文献
Jefford, Charles W.; Estrada, Manuel Jimenez; Barchietto, Giacomo; Berclaz, Theo; Geoffroy, Michel
Helvetica Chimica Acta, 1990 , vol. 73, # 6 p. 1653 - 1658
反应条件
oxygen; ethenetetracarbonitrile in dichloromethane 7 h; Irradiationwithout tetracyanoethylene, var. time;
参考文献
Nelsen, Stephen F.; Teasley, Mark F.
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3474 - 3479
反应条件
silica gel; ozone in tetrachloromethane T=20°C; further reagent;
参考文献
Voloshin, A. I.; Shapirov, G. L.; Kazkov, V. P.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 11 p. 2397 - 2399
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 11 p. 2613 - 2615
反应条件
pyridine; methanol in dichloromethane T=-78°C; 0.0833333 h; generation of singlet Oxygen;
参考文献
Bartlett, Paul D.; Mendenhall, G. David; Durham, Dana L.
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4269 - 4271
反应条件
oxygen; trifluoroacetic acid in dichloromethane 1 h;
参考文献
Akaba, Ryoichi; Sakuragi, Hirochika; Tokumaru, Katsumi
Tetrahedron Letters, 1984 , vol. 25, # 6 p. 665 - 668
反应条件
2.4E-3 M TPP(1+)*BF(1-); oxygen in dichloromethane 0.5 h; Ambient temperatureIrradiationdifferent reaction times and irradiation wavelength; Product distributionMechanism;
参考文献
Akaba, Ryoichi; Aihara, Shin; Sakuragi, Hirochika; Tokumaru, Katsumi
Journal of the Chemical Society, Chemical Communications, 1987 , # 16 p. 1262 - 1263
反应条件
methylene blue in dichloromethane T=15°C; 6 h; Irradiationvarious solvents, temperature, with or without SO2; Product distributionMechanism;
参考文献
Ando, Wataru; Sonobe, Hideki; Akasaka, Takeshi
Tetrahedron Letters, 1986 , vol. 27, # 37 p. 4473 - 4476
反应条件
in acetone 1) -78 deg C, 2) RT, 30 min.;
参考文献
Bartlett, Paul D.; Chu, Hsien-Kun
Journal of Organic Chemistry, 1980 , vol. 45, # 15 p. 3000 - 3004
反应条件
oxygen; Ledwith–Weitz salt in dichloromethane T=18°C; 10 h; other reagent, temperature, times, other adamantylidene compounds; Product distribution;
参考文献
Lopez, Luigi; Troisi, Luigino; Mele, Giuseppe
Tetrahedron Letters, 1991 , vol. 32, # 1 p. 117 - 120
反应条件
in benzene γ-radiolysis, other solvents;
参考文献
Sharipov, G. L.; Voloshin, A. I.; Khalilov, L. M.; Kazakov, V. P.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 9.2. p. 1993
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , vol. 39, # 9 p. 2183 - 2184