反应条件
1: 44 percent / LDA / tetrahydrofuran; hexane / 1.) -78 deg C, 30 min, 2.) -78 to 0 deg C 2: 98 percent / DIBAL / tetrahydrofuran / -78 °C 3: 10percent aq. HCl / 1,2-dichloro-ethane 4: 78 percent / DMPU, n-BuLi / tetrahydrofuran; hexane / 1.) 0 deg C, 20 min, 2.) -78 deg C, 60 min; -78 to 0 deg C 5: H2 / Rh(PPh3)Cl / benzene / 2 h / 25 °C 6: 5 N aq. NaOH / ethanol / Heating View Scheme
参考文献
Bennani; Boehm
Journal of Organic Chemistry, 1995 , vol. 60, # 5 p. 1195 - 1200
