2-氨基-4,6-二硝基甲苯合成路线 （共 32 条）
反应条件
1: 80percent aq. H2SO4, 90percent aq. nitric acid / 24 h / Ambient temperature 2: 78 percent / 96percent aq. H2SO4, anisole / 0.5 h / Ambient temperature 3: 40 percent / 90percent HNO3, 100percent H2SO4 / 1.) RT, 60 min, 2.) 75 deg C, 90 min 4: 97 percent / anh. ammonia / toluene; CCl4 / 0.58 h View Scheme
参考文献
Atkins, Ronald L.; Hollins, Richard A.; Wilson, William S.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3261 - 3266
反应条件
Diazotization.Erwaermen der Diazoniumsulfatloesung mit Alkohol;
参考文献
Holleman; Boeeseken
Recueil des Travaux Chimiques des Pays-Bas, 1897 , vol. 16, p. 426
反应条件
in tetrahydrofuran; N-methyl-acetamide
参考文献
May and Baker Limited
Patent: US3976786 A1, 1976 ;
反应条件
in pyridine 0.666667 h; Heating;
参考文献
Atkins, Ronald L.; Hollins, Richard A.; Wilson, William S.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3261 - 3266
参考文献
Lemberg; Callaghan
Australian Journal of Experimental Biology and Medical Science, 1945 , vol. 23, p. 6,9,10
反应条件
1: 0.6 g / 96percent aq. H2SO4, 100percent nitric acid / 24 h / Ambient temperature
2: 0.24 g / 96percent aq. H2SO4, 30percent oleum, 88percent aq. hydrogen peroxide / Ambient temperature
View Scheme
参考文献
Atkins, Ronald L.; Hollins, Richard A.; Wilson, William S.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3261 - 3266
反应条件
1: 0.6 g / 96percent aq. H2SO4, 100percent nitric acid / 24 h / Ambient temperature
2: 0.24 g / 96percent aq. H2SO4, 30percent oleum, 88percent aq. hydrogen peroxide / Ambient temperature
3: 74 percent / 0.4 N ammonia in dioxane / tetrahydrofuran / 0.17 h / Ambient temperature
View Scheme
参考文献
Atkins, Ronald L.; Hollins, Richard A.; Wilson, William S.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3261 - 3266
反应条件
Myriophyllum aquaticum in water
T=20°C; Reduction; 768 h; Enzymatic reaction; Product distributionKinetics;
参考文献
Bhadra; Spanggord; Wayment; Hughes; Shanks
Environmental Science and Technology, 1999 , vol. 33, # 19 p. 3354 - 3361
反应条件
1: 80percent aq. H2SO4, 90percent aq. nitric acid / 24 h / Ambient temperature
2: 78 percent / 96percent aq. H2SO4, anisole / 0.5 h / Ambient temperature
View Scheme
参考文献
Atkins, Ronald L.; Hollins, Richard A.; Wilson, William S.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3261 - 3266
反应条件
sulfuric acid; nitric acid
24 h; Ambient temperature;
参考文献
Atkins, Ronald L.; Hollins, Richard A.; Wilson, William S.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3261 - 3266
