1-甲基-2-苯基吲哚合成路线 (共 124 条)
反应条件
in dichloromethane
48 h; Ambient temperature;
参考文献
Berti, Corrado; Colonna, Martino; Poloni, Marino
Gazzetta Chimica Italiana, 1986 , vol. 116, # 4 p. 181 - 184
反应条件
in benzene
T=140°C; 14 h; Product distribution;
参考文献
Bruni, Paolo; Conti, Carla; Tosi, Giorgio
Monatshefte fuer Chemie, 1988 , vol. 119, p. 1311 - 1316
反应条件
1: 30 percent / lead tetra-acetate / CH2Cl2 / 5 h / Ambient temperature
2: 42 percent / KOH / ethanol; H2O / 4 h / Heating
View Scheme
参考文献
Sukari, Mohamed A.; Vernon, John M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2219 - 2224
反应条件
trans-[Pt(μ-Cl)Cl(C2H4)]2 in 1,4-dioxane
T=90°C; P=2585.74 Torr;
参考文献
Zhang, Zhibin; Wang, Xiang; Widenhoefer, Ross A.
Chemical Communications, 2006 , # 35 p. 3717 - 3719
反应条件
sodium hydrogencarbonate; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate); potassium iodide in toluene
T=20°C; 2 h; Schlenk technique; Reagent/catalyst; regioselective reaction;
参考文献
Shi, Leilei; Zhang, Dongmei; Lin, Riyuan; Zhang, Chun; Li, Xun; Jiao, Ning
Tetrahedron Letters, 2014 , vol. 55, # 14 p. 2243 - 2245
反应条件
tertiary butyl peroxybenzenoate; palladium (II) trifluoroacetate; acetic acid in 1,4-dioxane-d8
T=26.84°C; Inert atmosphere; Kinetics;
参考文献
Nimje, Roshan Y.; Leskinen, Mikko V.; Pihko, Petri M.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 18 p. 4818 - 4822
Angew. Chem., 2013 , vol. 125, # 18 p. 4918 - 4922,5
反应条件
dimethylaluminum chloride in hexane; toluene
T=20°C; Friedel-Crafts reaction; P=22502.3 Torr; 3 h; regioselective reaction;
参考文献
Nemoto, Koji; Onozawa, Satoru; Egusa, Naoki; Morohashi, Naoya; Hattori, Tetsutaro
Tetrahedron Letters, 2009 , vol. 50, # 31 p. 4512 - 4514
反应条件
N-nitroso-diphenylamine; trichloroacetic acid in dichloromethane
1 h; Ambient temperature;
参考文献
Cardellini; Greci; Stipa
Synthetic Communications, 1994 , vol. 24, # 5 p. 677 - 682
反应条件
dinitrogen tetraoxide in benzene
T=20°C; 0.166667 h;
参考文献
Astolfi, Paola; Panagiotaki, Maria; Rizzoli, Corrado; Greci, Lucedio
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 17 p. 3282 - 3290
反应条件
acetic acid; sodium nitrite in benzene
4 h;
参考文献
Astolfi, Paola; Panagiotaki, Maria; Rizzoli, Corrado; Greci, Lucedio
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 17 p. 3282 - 3290