1-甲基-2-苯基吲哚合成路线 （共 124 条）
反应条件
1: With zinc trifluoromethanesulfonate T=20°C; 1 h; Inert atmosphere; 2: With 1,1'-bis-(diphenylphosphino)ferrocene; tri-ruthenium(0)dodecacarbonyl; toluene-4-sulfonic acid in 1,4-dioxane T=150°C; 22 h; Inert atmosphere; regioselective reaction;
参考文献
Pena-Lopez, Miguel; Neumann, Helfried; Beller, Matthias
Chemistry - A European Journal, 2014 , vol. 20, # 7 p. 1818 - 1824
反应条件
palladium diacetate in tetrahydrofuran T=20°C; 24 h;
参考文献
Yang, Qi; Chang, Jiao; Wu, Qun; Zhang, Bianxiang
Research on Chemical Intermediates, 2012 , vol. 38, # 7 p. 1335 - 1340
反应条件
dichloro(cycloocta-1,5-diene)palladium(II); CuCl2·2H2O in 1,4-dioxane; toluene T=110°C; 24 h; Inert atmosphere;
参考文献
Wu, Mingyue; Luo, Jiaying; Xiao, Fuhong; Zhang, Shufeng; Deng, Guo-Jun; Luo, He-An
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 335 - 340
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=0°C; Inert atmosphere; 2: With water in tetrahydrofuran; hexane T=0 - 25°C; Inert atmosphere;
参考文献
Speranca, Adriane; Godoi, Benhur; Menezes, Paulo Henrique; Zeni, Gilson
Synlett, 2013 , vol. 24, # 9 art. no. ST-2013-S0135-L, p. 1125 - 1132
反应条件
1: 1-methyl-1H-indole With tert.-butyl lithium in tetrahydrofuran; pentane T=20°C; 2: in tetrahydrofuran; pentane T=-20°C; 3: [(C6H5)2l]CI in tetrahydrofuran; pentane T=-20 - 20°C;
参考文献
Ishikura, Minoru; Uemura, Reina; Yamada, Koji; Yanada, Reiko
Heterocycles, 2006 , vol. 68, # 11 p. 2349 - 2356
反应条件
C46H48N6O5Pd; potassium acetate in N,N-dimethyl acetamide T=160°C; 24 h; Inert atmosphere;
参考文献
Nandi, Debkumar; Jhou, Yang-Ming; Lee, Jhen-Yi; Kuo, Bing-Chiuan; Liu, Chien-Yu; Huang, Pei-Wen; Lee, Hon Man
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9384 - 9390
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene T=90°C; 28 h; Product distribution; Further Variations:TemperaturesSolventsPressuresReagentsreaction times; microwave irradiation;
参考文献
Shieh, Wen-Chung; Dell, Steven; Repic, Oljan
Organic Letters, 2001 , vol. 3, # 26 p. 4279 - 4281
反应条件
1: Pd(PPh3)4; Et2NH; CuI / dimethylformamide / 40 °C 2: PtCl2 / methoxybenzene / 2 h / 80 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 126, # 34 p. 10546 - 10547
反应条件
C46H48N6O5Pd; potassium acetate in N,N-dimethyl acetamide T=160°C; 24 h; Inert atmosphere;
参考文献
Nandi, Debkumar; Jhou, Yang-Ming; Lee, Jhen-Yi; Kuo, Bing-Chiuan; Liu, Chien-Yu; Huang, Pei-Wen; Lee, Hon Man
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9384 - 9390
反应条件
caesium acetate in N,N-dimethyl acetamide T=120°C; 24 h;
参考文献
Chemical Communications, , vol. 47, # 2 p. 806 - 808
