1-甲基-2-苯基吲哚合成路线 （共 124 条）
反应条件
methylammonium sulfite; methylamine in ethanol; water T=175°C; 30 h;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 26, # 9 p. 1016 - 1022
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 26, # 9 p. 1217 - 1225
反应条件
1.1: 96 percent / CuI; Et3N; PdCl2(PPh3)2 / tetrahydrofuran / 2 h / 20 °C 2.1: KH / 1-methyl-pyrrolidin-2-one / 2 h / 20 °C 2.2: 96 percent / 1-methyl-pyrrolidin-2-one / 0.5 h View Scheme
参考文献
Tetrahedron, , vol. 59, # 9 p. 1571 - 1587
反应条件
sodium hydroxide 60 degC 30 min then 80-90 degC 1 h;
参考文献
Colonna, Martino; Greci, Lucedio; Poloni, Marino
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 628 - 632
反应条件
1: 64 percent / sodium acetate / acetic acid / 3 h / Ambient temperature 2: 84 percent / thiosalicylic acid / trifluoroacetic acid / 1.5 h / 72 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 59, # 21 p. 6372 - 6377
反应条件
1: 64 percent / sodium acetate / acetic acid / 3 h / Ambient temperature 2: 84 percent / thiosalicylic acid / trifluoroacetic acid / 1.5 h / 72 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 59, # 21 p. 6372 - 6377
反应条件
Pd2[(C6H4)PPh2]2[CF3C(O)CHC(O)CF3]2 in acetic acid T=24.84°C; 30 h; Inert atmosphereSchlenk technique; Catalytic behavior; Reagent/catalystTimeSolvent;
参考文献
Ibanez, Susana; Estevan, Francisco; Hirva, Pipsa; Sanau, Mercedes; Ubeda, Ma. Angeles
Organometallics, 2012 , vol. 31, # 23 p. 8098 - 8108
反应条件
1: |Acidic conditions 2: palladium dichloride; silver(I) acetate; sulfuric acid / N,N-dimethyl-formamide; acetonitrile / 0.67 h / 100 °C / |Sealed tube; |Microwave irradiation View Scheme
参考文献
Chemistry - An Asian Journal, , vol. 8, # 12 p. 3185 - 3190
反应条件
zinc(II) chloride T=180°C;
参考文献
Chemische Berichte, , vol. 21, p. 2197
Chemische Berichte, , vol. 21, p. 2595
反应条件
in pyridine 4 h; Heating;
参考文献
Bergman, Jan; Eklund, Nils
Tetrahedron, 1980 , vol. 36, p. 1439 - 1443
反应条件
tert.-butyl lithium; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 3 h; Heating; Product distribution;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 2 p. 135 - 136
