1-甲基-2-苯基吲哚合成路线 （共 124 条）
反应条件
tert.-butyl lithium; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 3 h; Heatingother catalysts; other temp./reaction time; Product distribution;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 2 p. 135 - 136
反应条件
caesium acetate in N,N-dimethyl-formamide T=140°C; 48 h; Overall yield = 70 percent;
参考文献
Angewandte Chemie - International Edition, , vol. 53, # 1 p. 127 - 131
Angew. Chem., , vol. 126, # 01 p. 5131 - 5135
反应条件
triethyl borane; tert.-butyl lithium; bis-triphenylphosphine-palladium(II) chloride 1.) THF, pentane, hexane, r.t., 1 h; -20 deg C, 1 h, 2.) xylene, CO, 15 atm., 90 deg C, 60 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 59, # 9 p. 2634 - 2637
反应条件
triethyl borane; tert.-butyl lithium; bis-triphenylphosphine-palladium(II) chloride 1.) THF, pentane, hexane, r.t., 1 h; -20 deg C, 1 h, 2.) THF, CO, 1 atm., reflux, 20 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 59, # 9 p. 2634 - 2637
反应条件
magnesium bromide; [1,4-bis-(diphenylphosphine)butane]palladium (II) dichloride 1.-) THF, ether, room temp. 2.) reflux, 15 min.; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 22, # 52 p. 5319 - 5322
反应条件
1: 89 percent / 24 h 2: 8 percent / MeNH2 / 30 h / 150 °C View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 26, # 9 p. 1016 - 1022
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 26, # 9 p. 1217 - 1225
反应条件
1: 80 percent / NaBH4 / tetrahydrofuran / 10 h / 20 °C View Scheme
参考文献
Heterocycles, , vol. 30, # 1 p. 407 - 414
反应条件
1: 85 percent / ethanol / 20 °C 2: 80 percent / NaBH4 / tetrahydrofuran / 10 h / 20 °C View Scheme
参考文献
Heterocycles, , vol. 30, # 1 p. 407 - 414
反应条件
zinc(II) chloride T=220°C;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 253, p. 42
反应条件
hydrogenchloride T=100°C;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 253, p. 23
