1-甲基-2-苯基吲哚合成路线 （共 124 条）
反应条件
triethyl borane; tert.-butyl lithium; bis-triphenylphosphine-palladium(II) chloride 1.) THF, pentane, hexane, r.t., 1 h; -20 deg C, 1 h, 2.) xylene, 15 atm., 90 deg C, 60 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 59, # 9 p. 2634 - 2637
反应条件
methylamine T=150°C; 30 h;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 26, # 9 p. 1016 - 1022
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 26, # 9 p. 1217 - 1225
反应条件
hydrogen bromide 7 h; Heating;
参考文献
Bansal, Raj Kumar; Bhagchandani, Gope
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 8 p. 2423 - 2424
反应条件
in N,N-dimethyl-formamide T=80°C; 20 h;
参考文献
Suvorov, N. N.; Plutitskii, D. N.; Smushkevich, Yu. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 3 p. 268 - 270
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , vol. 17, # 3 p. 365 - 367
反应条件
1.1: anhydrous iron chloride / dichloromethane / 0.33 h / 25 °C 1.2: air / 24 h / 25 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 0 °C / |Inert atmosphere 2.2: 0 - 25 °C / |Inert atmosphere View Scheme
参考文献
Synlett, , vol. 24, # 9 art. no. ST-2013-S0135-L, p. 1125 - 1132
反应条件
1: With phosphoric acid T=20°C; Fishecher indole synthesis; 0.5 h; 2: T=20 - 120°C; Fishecher indole synthesis;
参考文献
Chemistry - A European Journal, , vol. 16, # 27 p. 7996 - 8001
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 8 p. 2423 - 2424
反应条件
ammonia; sodium amide und anschliessend mit Methyljodid;
参考文献
Journal of the Chemical Society, , p. 3388,3396
反应条件
2: zinc chloride / 180 °C View Scheme
参考文献
Chemische Berichte, , vol. 21, p. 2595
反应条件
hydrogenchloride; tetra-n-butylammonium perchlorate 1.) electrolysis at -2.77 V, DMF, H2O, 21.0 deg C, 2.) EtOH; Yield given. Multistep reaction;
参考文献
Journal of Chemical Research, Miniprint, , # 11 p. 3944 - 3965
