(2,2-二甲基苯并二氢吡喃-8-基)甲醇合成路线 （共 3 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C;
参考文献
Metabolex, Inc.
Patent: US2011/313003 A1, 2011 ;
Location in patent: Page/Page column 26-27 ;
US 20110313003 A1
反应条件
1.1: sulfuric acid; acetic acid / 0.75 h / 100 °C 2.1: n-butyllithium / diethyl ether; hexanes / 1.5 h / Reflux 2.2: 20 °C 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.17 h / 0 - 20 °C / Inert atmosphere 3.2: 0 °C View Scheme
参考文献
Metabolex, Inc.
Patent: US2011/313003 A1, 2011 ;
US 20110313003 A1
反应条件
1.1: n-butyllithium / diethyl ether; hexanes / 1.5 h / Reflux 1.2: 20 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.17 h / 0 - 20 °C / Inert atmosphere 2.2: 0 °C View Scheme
参考文献
Metabolex, Inc.
Patent: US2011/313003 A1, 2011 ;
US 20110313003 A1
