4-甲氧基-2-甲基苯甲酸甲酯合成路线 (共 27 条)
反应条件
1: 42 percent / AlCl3 2: 64 percent / Br2, aq. NaOH / 0.5 h / 40 °C 3: 73 percent / conc. H2SO4 / 24 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 30, # 10 p. 1798 - 1806
反应条件
in diethyl ether T=23°C; Irradiation; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 25, # 21 p. 2201 - 2204
反应条件
in diethyl ether T=23°C; Irradiation; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 25, # 21 p. 2201 - 2204
反应条件
in methanol T=65°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Helvetica Chimica Acta, , vol. 81, # 2 p. 251 - 267
反应条件
1: 1.) sec-BuLi, N,N,N',N'-tetramethylethylenediamine (TMEDA) / 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 2 h 2: 71 percent / concd. H2SO4 / 12 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 19 p. 3566 - 3572
反应条件
T=140 - 150°C; im geschlossenen Rohr;
参考文献
Chemische Berichte, , vol. 12, p. 818,821
参考文献
Bulletin de la Societe Scientifique de Bretagne, , vol. 31, p. Sonderheft S.9,41
反应条件
sodium hydrogencarbonate
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 23, # 1 p. 360 - 365
反应条件
T=200°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 120, p. 1339 - 1346
反应条件
in diethyl ether T=23°C; Irradiation; Rate constant;
参考文献
Tetrahedron Letters, , vol. 25, # 21 p. 2201 - 2204