4-(3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛基)苄醇 合成路线 （共 5 条）
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反应条件
356055-76-0 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛基)苄醇
反应条件
lithium aluminium tetrahydride in diethyl ether T=0 - 5°C;
参考文献
Curran, Dennis P.; Amatore, Muriel; Guthrie, David; Campbell, Matthew; Go, Eisan; Luo, Zhiyong
→
反应条件
356055-76-0 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛基)苄醇
反应条件
1.1: Zn; 1,2-dibromoethane; TMSCl / tetrahydrofuran / 15 h / 20 °C 1.2: 48 percent / tetrahydrofuran / 12 h / 45 °C 2.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -40 °C 3.1: 0.366 g / NaBH4 / ethanol / 16 h / 25 °C View Scheme
参考文献
Curran, Dennis P.; Oderaotoshi, Yoji
→
反应条件
356055-76-0 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛基)苄醇
反应条件
1.1: Zn; 1,2-dibromoethane; TMSCl / tetrahydrofuran / 15 h / 20 °C 1.2: 48 percent / tetrahydrofuran / 12 h / 45 °C 2.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -40 °C 3.1: 0.366 g / NaBH4 / ethanol / 16 h / 25 °C View Scheme
参考文献
Curran, Dennis P.; Oderaotoshi, Yoji
→
反应条件
356055-76-0 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛基)苄醇
反应条件
1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -40 °C 2: 0.366 g / NaBH4 / ethanol / 16 h / 25 °C View Scheme
参考文献
Curran, Dennis P.; Oderaotoshi, Yoji
356055-76-0 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛基)苄醇
→
反应条件
556050-48-7 N-[4-(3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛基)苄氧基羰酰氧基]琥珀酰亚胺
反应条件
1: phosgene; 4-(1H,1H,2H,2H-perfluorooctyl)benzyl alcohol in tetrahydrofuran; toluene
T=20°C;
2: dicyclohexylamine salt of N-hydroxysuccinimide in chloroform
T=20°C;
参考文献
Curran, Dennis P.; Amatore, Muriel; Guthrie, David; Campbell, Matthew; Go, Eisan; Luo, Zhiyong
