2-(9-氧代氧杂蒽-4-基)乙酸合成路线 （共 9 条）
反应条件
1: Cs2CO3; tris[2-(2-methoxyethoxy)ethyl]amine; CuCl / dioxane / 20 h / Heating 2: sulfuric acid / 1 h / 85 °C View Scheme
参考文献
Blake, Jessie A.; Gagnon, Eric; Lukeman, Matthew; Scaiano
Organic Letters, 2006 , vol. 8, # 6 p. 1057 - 1060
反应条件
1: Cs2CO3; tris[2-(2-methoxyethoxy)ethyl]amine; CuCl / dioxane / 20 h / Heating 2: sulfuric acid / 1 h / 85 °C View Scheme
参考文献
Blake, Jessie A.; Gagnon, Eric; Lukeman, Matthew; Scaiano
Organic Letters, 2006 , vol. 8, # 6 p. 1057 - 1060
反应条件
sulfuric acid; water; acetic acid T=80°C;
参考文献
Rewcastle, Gordon W.; Atwell, Graham J.; Baguley, Bruce C.; Calveley, Stephen B.; Denny, William A.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 4 p. 793 - 799
反应条件
1: N-bromosuccinimide, (PhCO)2O2 / CCl4 / Heating; Irradiation 2: ethanol; H2O / Heating 3: conc. H2SO4, AcOH, H2O / 80 °C View Scheme
参考文献
Rewcastle, Gordon W.; Atwell, Graham J.; Baguley, Bruce C.; Calveley, Stephen B.; Denny, William A.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 4 p. 793 - 799
反应条件
1: ethanol; H2O / Heating 2: conc. H2SO4, AcOH, H2O / 80 °C View Scheme
参考文献
Rewcastle, Gordon W.; Atwell, Graham J.; Baguley, Bruce C.; Calveley, Stephen B.; Denny, William A.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 4 p. 793 - 799
反应条件
acetic acid 3.2 h; Heating; Further byproducts given. Title compound not separated from byproducts;
参考文献
Nishino, Hiroshi; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2847 - 2848
反应条件
acetic acid 3.2 h; Heating; Further byproducts given;
参考文献
Nishino, Hiroshi; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2847 - 2848
反应条件
acetic acid 3.2 h; Heating; Further byproducts given;
参考文献
Nishino, Hiroshi; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2847 - 2848
反应条件
phosphate buffer in water
pH=7.4; Irradiation; Quantum yieldKinetics;
参考文献
Blake, Jessie A.; Gagnon, Eric; Lukeman, Matthew; Scaiano
Organic Letters, 2006 , vol. 8, # 6 p. 1057 - 1060
