2,2'-[1,4-亚苯基二(氧基-2,1-乙二基氧基)]二乙醇合成路线 （共 6 条）
反应条件
potassium carbonate 1.) DMF, 30 min, 2.) DMF, 75 deg C, 7 d; Yield given. Multistep reaction;
参考文献
Wu, Yuanzhao; Dong, Yu; Li, Junfeng; Huang, Xiaobo; Cheng, Yixiang; Zhu, Chengjian
Chemistry - An Asian Journal, 2011 , vol. 6, # 10 p. 2725 - 2729
反应条件
1: NaOH, sodium dithionite / butan-1-ol / 30 h / Heating 2: conc. HCl / methanol; CH2Cl2 / 4 h / Ambient temperature View Scheme
参考文献
Gibson, Harry W.; Nagvekar, Devdatt S.; Delaviz, Yadollah; Bryant, William S.
Canadian Journal of Chemistry, 1998 , vol. 76, # 10 p. 1429 - 1436
反应条件
1: 88 percent / triethylamine / CH2Cl2 / 15 h / Ambient temperature 2: 1.) NaH / 1.) THF, 1 h, 2.) THF, reflux 4 d View Scheme
参考文献
Anelli, Pier Lucio; Ashton, Peter R.; Ballardini, Roberto; Balzani, Vincenzo; Delgado, Milagros; Gandoffi, Maria Teresa; Goodnow, Timothy T.; Kaifer, Angel E.; Philp, Douglas; Pietraszkiewicz, Marek; Prodi, Luca; Reddington, Mark V.; Slawin, Alexandra M.Z.; Spencer, Neil; Fraser Stoddart; Vicent, Cristina; Williams, David J.
Journal of the American Chemical Society, 1992 , vol. 114, # 1 p. 193 - 218
反应条件
sodium hydride 1.) THF, 1 h, 2.) THF, reflux 4 d; Yield given. Multistep reaction;
参考文献
Anelli, Pier Lucio; Ashton, Peter R.; Ballardini, Roberto; Balzani, Vincenzo; Delgado, Milagros; Gandoffi, Maria Teresa; Goodnow, Timothy T.; Kaifer, Angel E.; Philp, Douglas; Pietraszkiewicz, Marek; Prodi, Luca; Reddington, Mark V.; Slawin, Alexandra M.Z.; Spencer, Neil; Fraser Stoddart; Vicent, Cristina; Williams, David J.
Journal of the American Chemical Society, 1992 , vol. 114, # 1 p. 193 - 218
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane 12 h;
参考文献
Ballardini; Balzani; Credi; Gandolfi; Marquis; Perez-Garcia; Stoddart
European Journal of Organic Chemistry, 1998 , # 1 p. 81 - 89
反应条件
pyridine; thionyl chloride in toluene
24 h; Heating;
参考文献
Gibson, Harry W.; Nagvekar, Devdatt S.; Delaviz, Yadollah; Bryant, William S.
Canadian Journal of Chemistry, 1998 , vol. 76, # 10 p. 1429 - 1436
