4-甲基苄基硼酸频哪醇酯合成路线 (共 16 条)
反应条件
magnesium; triethylamine in tetrahydrofuran Barbier-type reaction; 15 h; Inert atmosphereReflux;
参考文献
Pintaric, Christine; Olivero, Sandra; Gimbert, Yves; Chavant, Pierre Y.; Dunach, Elisabet
Journal of the American Chemical Society, 2010 , vol. 132, # 34 p. 11825 - 11827
反应条件
Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=25°C; Suzuki-Miyaura coupling; 5 h; Inert atmosphere; chemoselective reaction;
参考文献
Endo, Kohei; Ohkubo, Takahiro; Shibata, Takanori
Organic Letters, 2011 , vol. 13, # 13 p. 3368 - 3371
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in 1,4-dioxane T=100°C; Suzuki cross-coupling reaction; 18 h;
参考文献
Giroux, Andre
Tetrahedron Letters, 2003 , vol. 44, # 2 p. 233 - 235
反应条件
lithium bis((trifluoromethyl)sulfonyl)amide in tetrahydrofuran T=20°C; Electrochemical reaction;
参考文献
Pintaric; Laza; Olivero; Dunach
Tetrahedron Letters, 2004 , vol. 45, # 43 p. 8031 - 8033
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in 1,4-dioxane T=80°C; Suzuki cross-coupling reaction; 6 h;
参考文献
Giroux, Andre
Tetrahedron Letters, 2003 , vol. 44, # 2 p. 233 - 235
反应条件
palladium on activated charcoal in xylene byproducts: H2; 16 h at 100°C under N2; catalyst: 10percent Pd/C (3 molpercent);
参考文献
Ishiyama, Tatsuo; Ishida, Kousaku; Takagi, Jun; Miyaura, Norio
Chemistry Letters, 2001 , # 11 p. 1082 - 1083
反应条件
palladium on activated charcoal T=100°C; 16 h;
参考文献
Ishiyama, Tatsuo; Ishida, Kousaku; Takagi, Jun; Miyaura, Norio
Chemistry Letters, 2001 , # 11 p. 1082 - 1083
反应条件
trans-chloro(dinitrogen)bis(tri-isopropylphosphine)rhodium(I) in xylene hated at 140°C for 80 h;
参考文献
Angewandte Chemie - International Edition, , vol. 40, # 11 p. 2168 - 2171
反应条件
sodium methylate in methanol; toluene T=90°C; Inert atmosphere;
参考文献
Li, Huan; Wang, Long; Zhang, Yan; Wang, Jianbo
Angewandte Chemie - International Edition, 2012 , vol. 51, # 12 p. 2943 - 2946
反应条件
Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water T=60°C; Suzuki-Miyaura Coupling; 5 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 17 p. 7223 - 7231