4-甲基苄基硼酸频哪醇酯合成路线 （共 16 条）
反应条件
1: methanol / 70 °C / Inert atmosphere 2: sodium methylate / methanol; toluene / 90 °C / Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 12 p. 2943 - 2946
反应条件
NaOMe in methanol; toluene 90°C, 3-12 h;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 12 p. 2943 - 2946
反应条件
PdCl2(dpff); potassium carbonate in N,N-dimethyl-formamide T=80°C; 18 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Tetrahedron Letters, , vol. 44, # 2 p. 233 - 235
反应条件
1: 4-methylbenzylboronic pinacol ester With Pd0(tris(tert-butyl)phosphine)2; cesium fluoride in water; N,N-dimethyl-formamide T=80°C; 0.0166667 h; Inert atmosphereSchlenk technique; 2: methyl iodide in water; N,N-dimethyl-formamide T=80°C; 0.0833333 h; Inert atmosphereSchlenk technique;
参考文献
RSC Advances, , vol. 3, # 24 p. 9391 - 9401
反应条件
potassium bifluoride in tetrahydrofuran; water T=20°C;
参考文献
Yasu, Yusuke; Koike, Takashi; Akita, Munetaka
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 18 p. 3414 - 3420
反应条件
1: 4-methoxy-aniline; PhCH2Bpin With di-tert-butyl peroxide; copper diacetate in toluene T=50°C; 24 h; Sealed tubeInert atmosphere; 2: 4-methylbenzylboronic pinacol ester in toluene T=100°C; 24 h; Sealed tubeInert atmosphere;
参考文献
Organic Letters, , vol. 15, # 7 p. 1544 - 1547
