(E)-2-甲基-2-丁烯酰氯合成路线 （共 51 条）
反应条件
phenyllithium
1.) dioxane-ether, -20 deg C; Yield given. Multistep reaction;
参考文献
Kubo; Nakahara
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 2 p. 595 - 596
反应条件
1: 84.6 percent / SnCl4 / CH2Cl2 / Ambient temperature
2: 86.9 percent / PPA / 2.5 h / 90 - 100 °C
View Scheme
参考文献
Carter, Rachel H.; Garson, Mary J.; Hill, Robert A.; Staunton, James; Sunter, David C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 471 - 479
反应条件
2: 53 percent / toluene / 19 h / 160 °C
View Scheme
参考文献
Danheiser, Rick L.; Gee, Stephen K.; Sard, Howard
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7670 - 7672
参考文献
Jackson, David A.; Rey, Max; Dreiding, Andre S.
Helvetica Chimica Acta, 1983 , vol. 66, # 7 p. 2330 - 2341
反应条件
in Petroleum ether
T=-60°C; 1 h;
参考文献
Lindner, Ekkehard; Tamoutsidis, Efstathios
Chemische Berichte, 1983 , vol. 116, # 9 p. 3141 - 3150
反应条件
1) -196 deg C to r.t., 2) 2 h, r.t.;
参考文献
Lindner, Ekkehard; Tamoutsidis, Efstathios
Chemische Berichte, 1983 , vol. 116, # 9 p. 3141 - 3150
参考文献
Jackson, David A.; Rey, Max; Dreiding, Andre S.
Tetrahedron Letters, 1983 , vol. 24, # 44 p. 4817 - 4820
反应条件
1: Et3N
2: 79 percent / neat (no solvent) / 4 h / 150 °C
View Scheme
参考文献
Jackson, David A.; Rey, Max; Dreiding, Andre S.
Helvetica Chimica Acta, 1983 , vol. 66, # 7 p. 2330 - 2341
反应条件
in neat (no solvent)
T=150°C; 4 h;
参考文献
Jackson, David A.; Rey, Max; Dreiding, Andre S.
Helvetica Chimica Acta, 1983 , vol. 66, # 7 p. 2330 - 2341
参考文献
Jackson, David A.; Rey, Max; Dreiding, Andre S.
Tetrahedron Letters, 1983 , vol. 24, # 44 p. 4817 - 4820
