(E)-2-甲基-2-丁烯酰氯合成路线 （共 51 条）
反应条件
triethylamine in neat (no solvent)
T=150°C; 4 h; other temperatures, other times, also with solvents; Product distribution;
参考文献
Jackson, David A.; Rey, Max; Dreiding, Andre S.
Helvetica Chimica Acta, 1983 , vol. 66, # 7 p. 2330 - 2341
反应条件
1: Et3N
2: 42 percent / 4 h / 150 °C
View Scheme
参考文献
Jackson, David A.; Rey, Max; Dreiding, Andre S.
Helvetica Chimica Acta, 1983 , vol. 66, # 7 p. 2330 - 2341
反应条件
1: 42 percent / triethylamine
2: 66 percent / CH3SO3H / CH2Cl2 / Ambient temperature
View Scheme
参考文献
Jackson, David A.; Rey, Max; Dreiding, Andre S.
Tetrahedron Letters, 1983 , vol. 24, # 44 p. 4817 - 4820
反应条件
1: 40 percent / triethylamine
2: 51 percent / CH3SO3H / Ambient temperature
View Scheme
参考文献
Jackson, David A.; Rey, Max; Dreiding, Andre S.
Tetrahedron Letters, 1983 , vol. 24, # 44 p. 4817 - 4820
反应条件
1: Et3N
2: 12 percent / neat (no solvent) / 4 h / 150 °C
View Scheme
参考文献
Jackson, David A.; Rey, Max; Dreiding, Andre S.
Helvetica Chimica Acta, 1983 , vol. 66, # 7 p. 2330 - 2341
反应条件
1: 70 percent / 1.88 M phenyllithium / diethyl ether; benzene / 0.08 h
2: 59 percent / 10percent palladium on carbon / benzene / 48 h / Heating
View Scheme
参考文献
Kubo; Nakahara; Inaba; Kitahara
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 6 p. 2582 - 2584
参考文献
Roehnert,H.
Journal fuer Praktische Chemie (Leipzig), 1966 , vol. 32, p. 265 - 273
Full Text Show Details
Giani et al.
Farmaco, Edizione Scientifica, 1959 , vol. 14, p. 784,790
Full Text Show Details
Roehnert
Journal fuer Praktische Chemie (Leipzig), 1966 , vol. <4>32, p. 265,273
反应条件
1: 84 percent / AlCl3 / Heating
2: 86 percent / diethyl ether / Heating
3: 79 percent / p-TsOH / toluene / 5 h / Heating
View Scheme
参考文献
Gelin,R.; Chantegrel,B.
Bulletin de la Societe Chimique de France, 1971 , p. 2527 - 2544
参考文献
Barger et al.
Journal of the Chemical Society, 1937 , p. 1820,1823
反应条件
1: 60 percent / tetrahydrofuran / 1.) -30 deg C, 1 h, 2.) -30 deg C to room temp.
2: H2 / Pd/C
View Scheme
参考文献
Dubois, Jacques-Emile; Lion, Claude; Arouisse, Abdelmajid
Bulletin des Societes Chimiques Belges, 1984 , vol. 93, # 12 p. 1083 - 1088
