芴甲氧羰基-DL-丙氨酸合成路线 （共 11 条）
反应条件
sodium carbonate in acetonitrile T=20°C; 1.25 h;
参考文献
Hioki, Kazuhito; Kinugasa, Mizuho; Kishimoto, Michiko; Fujiwara, Miho; Tani, Shohei; Kunishima, Munetaka
Synthesis, 2006 , # 12 p. 1931 - 1933
反应条件
sodium carbonate in acetone T=0 - 20°C;
参考文献
Chen, Laizhong; Sun, Wei; Li, Jing; Liu, Zhenzhen; Ma, Zhao; Zhang, Wei; Du, Lupei; Xu, Wenfang; Fang, Hao; Li, Minyong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 2 p. 378 - 382
反应条件
ytterbium(III) triflate in nitromethane T=45 - 50°C; 5 h;
参考文献
Sridhar, P. Ramu; Sinha, Surajit; Chandrasekaran
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 1 p. 157 - 160
反应条件
1: 95 percent / Et3N / CH2Cl2 / 1 h / 20 °C 2: 96 percent / aq. Na2CO3 / acetonitrile / 1.25 h / 20 °C View Scheme
参考文献
Hioki, Kazuhito; Kinugasa, Mizuho; Kishimoto, Michiko; Fujiwara, Miho; Tani, Shohei; Kunishima, Munetaka
Synthesis, 2006 , # 12 p. 1931 - 1933
参考文献
Carpino,L.A.; Han,G.Y.
Journal of Organic Chemistry, 1972 , vol. 37, # 22 p. 3404 - 3409
反应条件
1.1: Fmoc-Cl; N-methylmorpholine / tetrahydrofuran / 0.17 h / -15 °C 1.2: 86 percent / tetrahydrofuran; diethyl ether / 0 - 20 °C 2.1: 80 percent / silver benzoate / dioxane; H2O / 0.02 h / microwave irradiation View Scheme
参考文献
Ellmerer-Mueller, Ernst P.; Broessner, Dagmar; Maslouh, Najib; Tako, Andreas
Helvetica Chimica Acta, 1998 , vol. 81, # 1 p. 59 - 65
反应条件
thionyl chloride in dichloromethane T=20°C;
参考文献
Chaume, Gregory; Simon, Julien; Caupene, Caroline; Lensen, Nathalie; Miclet, Emeric; Brigaud, Thierry
Journal of Organic Chemistry, 2013 , vol. 78, # 20 p. 10144 - 10153
反应条件
Multistep reaction.;
参考文献
Leonetti, Francesco; Capaldi, Carmelida; Pisani, Leonardo; Nicolotti, Orazio; Muncipinto, Giovanni; Stefanachi, Angela; Cellamare, Saverio; Caccia, Carla; Carotti, Angelo
Journal of Medicinal Chemistry, 2007 , vol. 50, # 20 p. 4909 - 4916
反应条件
1: With 1-propanephosphonic acid cyclic anhydride; N-ethyl-N,N-diisopropylamine in ethyl acetate T=0°C; 0.166667 h; 2: With sodium tetrahydroborate in water; ethyl acetate T=0°C;
参考文献
Nagendra; Madhu; Vishwanatha; Sureshbabu, Vommina V.
Tetrahedron Letters, 2012 , vol. 53, # 38 p. 5059 - 5063
参考文献
Bryant, Sharon D.; Guerrini, Remo; Salvadori, Severo; Bianchi, Clementina; Tomatis, Roberto; Attila, Martti; Lazarus, Lawrence H.
Journal of Medicinal Chemistry, 1997 , vol. 40, # 16 p. 2579 - 2587
