萘并[2,3-c]吖啶-5,8,14(13H)-三酮合成路线 （共 21 条）
反应条件
1: nitrobenzene; iodine; sulfuryl chloride 2: nitrobenzene; bromine / 160 - 170 °C 4: sodium bi chromate; glacial acetic acid 5: potassium acetate; copper acetate 6: concentrated sulfuric acid View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
1: nitrobenzene; bromine / 160 - 170 °C 3: sodium bi chromate; glacial acetic acid 4: potassium acetate; copper acetate 5: concentrated sulfuric acid View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
1: potassium acetate; copper acetate 2: concentrated sulfuric acid View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
1: hydrochloric acid; sodium chlorate 2: nitrobenzene; bromine / 160 - 170 °C 4: sodium bi chromate; glacial acetic acid 5: potassium acetate; copper acetate 6: concentrated sulfuric acid View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
1: sodium bi chromate; glacial acetic acid 2: potassium acetate; copper acetate 3: concentrated sulfuric acid View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
2: sodium bi chromate; glacial acetic acid 3: potassium acetate; copper acetate 4: concentrated sulfuric acid View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
1: hydrochloric acid; aqueous-sodium chlorate 2: potassium acetate; copper acetate; copper powder / 150 - 160 °C / weiteres Reagens: Isoamylalkohol 3: concentrated sulfuric acid / 100 - 110 °C View Scheme
参考文献
Ullmann; Ochsner
Justus Liebigs Annalen der Chemie, 1911 , vol. 381, p. 8
反应条件
1: copper powder; sodium carbonate; nitrobenzene / 220 - 230 °C 2: concentrated sulfuric acid / 100 - 110 °C View Scheme
参考文献
Ullmann; Ochsner
Justus Liebigs Annalen der Chemie, 1911 , vol. 381, p. 8
反应条件
1: potassium acetate; copper acetate; naphthalene 2: diluted NaOH-solution; Na2S2O4 / 40 - 50 °C / bei nachfolgendem Einleiten von Luft View Scheme
参考文献
Ullmann; Dootson
Chemische Berichte, 1918 , vol. 51, p. 14
反应条件
sulfuryl dichloride; iodine; nitrobenzene
T=150°C;
参考文献
Am.Cyanamid Co.
Patent: US2492802 , 1945 ;
