三甲氧基(4-甲氧苯基)硅烷合成路线 （共 32 条）
反应条件
tris(dibenzylideneacetone)dipalladium (0); N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine in N,N-dimethyl-formamide T=20°C; silylation;
参考文献
Journal of the American Chemical Society, , vol. 122, # 31 p. 7600 - 7601
反应条件
1: 1-bromo-4-methoxy-benzene With magnesium in tetrahydrofuran T=20°C; 2: orthosilicic acid tetramethyl ester in tetrahydrofuran T=-30 - 20°C; 13 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 24 p. 8305 - 8314
参考文献
Chemical Communications, , # 14 p. 1309 - 1310
反应条件
tetrabutyl ammonium fluoride; tris-(o-tolyl)phosphine; dichloro bis(acetonitrile) palladium(II) T=80°C; Hiyama cross-coupling reaction; 1 h;
参考文献
Synthesis, , # 6 p. 969 - 974
反应条件
copper diacetate; tetrabutyl ammonium fluoride; oxygen in N,N-dimethyl-formamide T=20°C; Arylation; 48 h;
参考文献
Lam, Patrick Y. S.; Deudon, Sophie; Averill, Kristin M.; Li, Renhua; He, Ming Y.; DeShong, Philip; Clark, Charles G.
Journal of the American Chemical Society, 2000 , vol. 122, # 31 p. 7600 - 7601
反应条件
NHC-Pd(II)-Im; tetrabutyl ammonium fluoride in toluene T=120°C; Hiyama reaction; 3 h; Inert atmosphere;
参考文献
Gu, Zheng-Song; Shao, Li-Xiong; Lu, Jian-Mei
Journal of Organometallic Chemistry, 2012 , vol. 700, p. 132 - 134
反应条件
NHC-Pd(II)-Im; tetrabutyl ammonium fluoride in toluene T=120°C; Hiyama reaction; 3 h; Inert atmosphere;
参考文献
Gu, Zheng-Song; Shao, Li-Xiong; Lu, Jian-Mei
Journal of Organometallic Chemistry, 2012 , vol. 700, p. 132 - 134
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; tert-butyl alcohol T=90°C; Hiyama coupling; Inert atmosphere;
参考文献
Zhang, Liang; Qing, Jiang; Yang, Pengyuan; Wu, Jie
Organic Letters, 2008 , vol. 10, # 21 p. 4971 - 4974
反应条件
1,4-diaza-bicyclo[2.2.2]octane; tetrabutyl ammonium fluoride; palladium diacetate in 1,4-dioxane T=80°C; Hiyama cross-coupling reaction; 4 h;
参考文献
Li, Jin-Heng; Deng, Chen-Liang; Liu, Wen-Jie; Xie, Ye-Xiang
Synthesis, 2005 , # 18 art. no. F08405SS, p. 3039 - 3044
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in N,N-dimethyl-formamide; acetonitrile T=100°C; Hiyama Coupling; 3 h; Inert atmosphereGreen chemistry;
参考文献
Zhang, Wei; Liu, Fang; Li, Ke; Zhao, Baoli
Applied Organometallic Chemistry, 2014 , vol. 28, # 5 p. 379 - 381
