2,2',3,3',4,4',5,5'-八氯联苯合成路线 （共 9 条）
反应条件
sodium hydroxide in tetrahydrofuran 5 h; Heating;
参考文献
Journal of Organometallic Chemistry, , vol. 381, # 3 p. 321 - 332
反应条件
1: 14 percent / SiCl4 / tetrahydrofuran / 1.) room temp., 3 h, 2.) reflux, 2 h 2: 6 percent / tetrahydrofuran / 16 h / Heating 3: 100 percent / 10percent aq. NaOH / tetrahydrofuran / 5 h / Heating View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 381, # 3 p. 321 - 332
反应条件
1: 6 percent / tetrahydrofuran / 16 h / Heating 2: 100 percent / 10percent aq. NaOH / tetrahydrofuran / 5 h / Heating View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 381, # 3 p. 321 - 332
反应条件
copper in N,N-dimethyl-formamide Ulman reaction; Heating;
参考文献
Chemosphere, , vol. 31, # 2 p. 2687 - 2705
反应条件
1: HNO3 2: Zn, aq. CuSO4 / acetic acid 3: (i) NaNO2, aq. H2SO4, (ii) CuCl, aq. HCl View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 686 - 691
反应条件
1: Zn, aq. CuSO4 / acetic acid 2: (i) NaNO2, aq. H2SO4, (ii) CuCl, aq. HCl View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 686 - 691
反应条件
1: (i) aq. HCl, (ii) NaNO2, (iii) CuCl, aq. HCl 2: HNO3 3: Zn, aq. CuSO4 / acetic acid 4: (i) NaNO2, aq. H2SO4, (ii) CuCl, aq. HCl View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 686 - 691
反应条件
isopentyl nitrite Cadogan modification of Gomberg-Bachman;
参考文献
Chemosphere, , vol. 31, # 2 p. 2687 - 2705
反应条件
(i) NaNO2, aq. H2SO4, (ii) CuCl, aq. HCl; Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 686 - 691
