2,3,4,5,6,7,8,8a-八氢-1H-萘-4a-醇合成路线 （共 47 条）
反应条件
chromium(VI) oxide; tetrabutylammonium (meta)periodate in dichloromethane; acetonitrile T=-40°C; 0.166667 h;
参考文献
Lee, Seongmin; Fuchs
Journal of the American Chemical Society, 2002 , vol. 124, # 47 p. 13978 - 13979
反应条件
methyl(trifluoromethyl)dioxirane in dichloromethane T=-22°C; 0.0833333 h; Yields of byproduct given;
参考文献
Mello, Rossella; Fiorentino, Michele; Fusco, Caterina; Curci, Ruggero
Journal of the American Chemical Society, 1989 , vol. 111, # 17 p. 6749 - 6757
反应条件
1: With sodium tetrahydroborate; boron trifluoride diethyl etherate in tetrahydrofuran T=0 - 20°C; Addition; 2.5 h; 2: With anhydrous potassium sulfate; potassium hydrogensulfate; oxone in water T=0 - 20°C; Oxidation;
参考文献
Pfizer Products Inc.
Patent: EP1167329 A2, 2002 ;
Location in patent: Page 7 ;
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=60°C; 15 h;
参考文献
Beckwith, Athelstan L.J.; Kazlauskas, Rymantas; Syner-Lyons, Mark R.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4718 - 4722
反应条件
hydrogen; nickel in ethanol
参考文献
Cope,A.C. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 4299 - 4307
反应条件
BF3OEt2; sodium borohydride in tetrahydrofuran; water
参考文献
Cai, Weiling; Ripin, David H.
Patent: US2002/49352 A1, 2002 ;
反应条件
oxygen; Co-Ce-NH4Br in acetic anhydride T=95°C; P=760 Torr; 1 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yazu, Kaumasa; Wakabayashi, Takeshige; Nakayama, Tetsuo
Chemistry Letters, 1986 , p. 1409 - 1412
反应条件
tert.-butylhydroperoxide in water; acetonitrile T=60°C; 24 h;
参考文献
Djernes, Katherine E.; Padilla, Melissa; Mettry, Magi; Young, Michael C.; Hooley, Richard J.
Chemical Communications, 2012 , vol. 48, # 94 p. 11576 - 11578
反应条件
perfluoro-cis-2-n-butyl-3-n-propyloxaziridine in monofluoro-trichloromethane Ambient temperature;
参考文献
DesMarteau, Darryl D.; Donadelli, Alessandro; Montanari, Vittorio; Petrov, Viacheslav A.; Resnati, Giuseppe
Journal of the American Chemical Society, 1993 , vol. 115, # 11 p. 4897 - 4898
参考文献
Murray, Robert W.; Jeyaraman, Ramasubbu; Mohan, Lily
Journal of the American Chemical Society, 1986 , vol. 108, # 9 p. 2470 - 2472
