potassium carbonate in dimethyl sulfoxide T=20°C; 8 h;

potassium carbonate in N,N-dimethyl-formamide T=50°C;

in ethyl acetate; N,N-dimethyl-formamide

1: C31H42N5O3PolSi With caesium carbonate in water; N,N-dimethyl-formamide T=20°C; Mitsunobu reaction; 2 h; solid phase reaction; 2: allyl alcohol With di-isopropyl azodicarboxylate; triphenylphosphine in dichloromethane T=20°C; Mitsunobu reaction; 20 h; Inert atmospheresolid phase reaction; 3: methanol With copper(II) bis(trifluoromethanesulfonate) T=20°C; 15 h; solid phase reaction;

perchloric acid; sodium percarbonate; vanadium pentoxide 3 h; Cooling;

sodium methylate

potassium hydroxide in methanol T=20°C; 10 h;

aniline; (π-allyl)palladium triflate based catalyst T=30°C; 0.333333 h;

potassium hydroxide in methanol T=20°C; 10 h;

1: 90 percent / 2,6-di-tert-butyl-4-methylphenol (BHT) / various solvent(s) / Heating 2: 87 percent / K2CO3 / acetone / Heating 3: 94 percent / 2,6-di-tert-butyl-4-methylphenol (BHT) / various solvent(s) / Heating 4: 97 percent / Et3N, DMAP / CH2Cl2 5: 90 percent / H2 / 5percent Rh/C / ethanol 6: 92 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C 7: 82 percent / Ph3P, DEAD / tetrahydrofuran / 0 °C 8: 93 percent / n-Bu4NF / tetrahydrofuran 9: K2CO3 / acetone / Heating 10: 1 N aq. NaOH / methanol View Scheme