1: 71 percent / Br2, HgO / various solvent(s) / 1 h / 85 - 90 °C 2: 48 percent / Li / diethyl ether / a) from -30 deg C to -10 deg C, 1.5 h, b) -10 deg C, 1 h 3: 98 percent / CF3COOH, Et3SiH / CH2Cl2 / 2 h / 5 °C View Scheme
参考文献
Lomas, John S.; Cordier, Christine; Briand, Sylvette
Journal of the Chemical Society. Perkin Transactions 2, 1996 , vol. 5, p. 865 - 870
1: 48 percent / Li / diethyl ether / a) from -30 deg C to -10 deg C, 1.5 h, b) -10 deg C, 1 h 2: 98 percent / CF3COOH, Et3SiH / CH2Cl2 / 2 h / 5 °C View Scheme
参考文献
Lomas, John S.; Cordier, Christine; Briand, Sylvette
Journal of the Chemical Society. Perkin Transactions 2, 1996 , vol. 5, p. 865 - 870
Lomas, John S.; Cordier, Christine; Briand, Sylvette; Vaissermann, Jacqueline
Journal of the Chemical Society. Perkin Transactions 2, 1996 , vol. 5, p. 871 - 876
