1,2-双(1,1,2,2-四氟乙氧基)乙烷合成路线 (共 3 条)
反应条件
potassium hydroxide in N,N-dimethyl-formamide -78 to 30...80 deg C;
参考文献
Sievert, Allen C.; Tong, Walter R.; Nappa, Mario J.
Journal of Fluorine Chemistry, 1991 , vol. 53, # 3 p. 397 - 418
反应条件
diethyl ether; sodium T=75°C;
参考文献
Coffman et al.
Journal of Organic Chemistry, 1949 , vol. 14, p. 751
Full Text Show Details
du Pont de Nemours and Co.
Patent: US2409274 , 1943 ;
反应条件
fluorine; NAF in 1,2,2-trifluoro-trichloroethane T=-15°C; 2.05 h; Irradiationwithout catalyst; also ethylene glycol diethyl ether; Product distribution;
参考文献
Sievert, Allen C.; Tong, Walter R.; Nappa, Mario J.
Journal of Fluorine Chemistry, 1991 , vol. 53, # 3 p. 397 - 418