(C6H5)3CBF4 in acetonitrile Kinetics; byproducts: (C2H5)3SnF, (C6H5)3CH; 25°C;
参考文献
Traylor, T. G.; Berwin, H. J.; Jerkunica, J. M.; Hall, M. L.
Pure and Applied Chemistry, 1972 , vol. 30, p. 599 - 606
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.2.4.7, page 73 - 76
Treichel, P. M.; Goodrich, R. A.
Inorganic Chemistry, 1965 , vol. 4, p. 1424 - 1428
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.2.4.7, page 73 - 76
potassium fluoride in ethanol; water addn. of org. compd. to Sn-compd. (vac.), sealing, reacting (room temp., 1 d), sepn. of org. compd. on filtration (Ar atmosphere), addn. of aq.-alcoholic soln. of KF;
参考文献
Shcherbakov, V. I.; Stolyarova, N. E.; D'yachkovskaya, O. S.; Kuzina, V. I.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 714 - 718
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 886 - 891
in neat (no solvent) byproducts: C4HF5; decompn. at 20°C;;
参考文献
Petrov, A. D.; Mironov, V. F.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1957 , p. 1491 - 1493
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Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.2.4, page 181 - 192
Petrov, A. D.; Mironov, V. F.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1957 , p. 1491 - 1493
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Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.2.4, page 181 - 192
in neat (no solvent) reaction of org. compd. and Sn-compd. (0°C, evaccuated ampoule, ratio 1:2), warming (room temp.); isolation as triethylfluorostannane;
参考文献
Shcherbakov, V. I.; Stolyarova, N. E.; D'yachkovskaya, O. S.; Kuzina, V. I.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 714 - 718
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 886 - 891
Zakharkin, L. I.; Okhlobystin, O. Yu.; Strunin, B. N.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1962 , p. 2002 - 2008
C.A., 1963 , vol. 58, p. 9131
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.2.4.8, page 76 - 79
in neat (no solvent)
reaction without solvent at -30°C and storing for 2 h at 20°C;;
参考文献
Neumann, W. P.; Niermann, H.
Liebigs Annalen der Chemie, 1962 , vol. 653, p. 164 - 172
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.2, page 19 - 20
